Analysis of doxorubicin and fullerenol in rat serum by micellar electrokinetic capillary chromatography
Rade Injac,
Miranda Sertić,
Nina Kočevar Glavač
Abstract:A new micellar electrokinetic capillary chromatographic (MEKC) method has been developed and optimized for simultaneous quantitation of doxorubicin (Dox) and fullerenol (Frl) in rat serum. The separation was carried out in a capillary (48.5–40 cm to the detector – 50 µm id fused-silica capillary with bubble cell, 150 µm) at an applied voltage of 25 kV and temperature of 25 °C. For the background electrolyte 10 mmol L–
1 borate buffer pH 9.3 plus 15 mmol L–1 phosphate buffer pH 7.0 (with the f… Show more
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