“…The characteristic chemical structures of MOT, LCE, nano-LCE, LCE-MOT and nano-LCE-MOT were characterised by FTIR spectroscopy in the wavenumber range of 4000–400 cm −1 . Figure 2 shows the FTIR spectrum of LCE, which features peaks that can be attributed to -OH bending (3366 cm −1 ), the –OH stretching vibration of -COOH (1462 cm −1 ) and the -C-O-C- stretching vibration of cellulose and hemicellulose (1050 cm −1 ) [ 41 ], while after nanosizing treatment, the absorption peaks were shifted to 3360, 1474 and 1037 cm −1 , respectively, and a new peak attributed to -C=O appeared at 1622 cm −1 [ 42 ], indicating that the active groups of lignocellulose were exposed after the nanosizing treatment. From the results shown in Figure 2 , it is inferred that the nanosizing treatment of LCE does not change its chemical structure, it only reduces its size to nanosized, thus enhancing its adsorption capacity toward Zn (II) from effluent.…”