An improved analyzer for measuring in-situ gas pressure in sealed quartz tube, and absolute and differential temperatures in heat treatments up to high temperatures
Abstract:The measurement of in-situ pressure in synthesis and decomposition experiments, carried out in sealed quartz tubes or ampoules, provides important information about the reactions that occur during the heat treatment processes. In this work, a thermobarometric differentialthermal analyzer (TBDTA) is detailed to perform measurements of in-situ pressure in sealed quartz ampoules, and absolute and differential temperatures in heat treatments up to 800 • C. The system can also operate, with certain precautions, abo… Show more
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