?he influence of thermally induced microstructural transformations on
magnetic properties of Fe72Cu1V4Si15B8 ribbon with combined
amorphous/nanocrystalline structure is presented. The experiments showed
that thermally induced structural changes are in correlation with the
appearance of magnetic hysteresis, i.e. with inverted hysteresis loops (IHL)
and exchange bias (EB) effects. It was found that the ratio of surface to
volume of a ribbon sample have an influence on hysteresis loop appearance.
The inverted hysteresis loops were observed for the 1.5 mm wide and 55 ?m
thick alloy samples shorter than 10 mm, but for the samples longer than 10
mm hysteresis loops were normal. With an increase of annealing temperature,
a shift of the hysteresis loops measured at room temperature was noticed.
The highest positive exchange bias field Heb was observed for the sample
annealed at 723 K, together with the lowest magnetic field at which the
changes from inverted to normal hysteresis loop occurred. Annealing at the
temperature of 823 K resulted in negative Heb.