Alkoxyalkanol Modified Ti(OCHMe<sub>2</sub>)<sub>4</sub>: Synthesis and Characterization of Novel [(OPr<sup>i</sup>)<sub>4-n</sub>Ti (OC<sub>2</sub>H<sub>4</sub>OR)<sub>n</sub>]
Abstract:Novel structural arrangements for alkoxyalkanol modified titanium tetraisopropoxide [(Ti(OPri)4, TPT] were obtained from stoichiometric reactions between TPT and alkoxyalkanols {HOCH2CH2OR,where R= Me, Et}. All the 1:1, 1:2, 1:3 and 1:4 reactions in refluxing benzene form mononuclear species [(OPri)4-nTi(OC2H4OR)n]. All these compounds can be purified by distillation under reduced pressure. On the basis of IR and NMR (1H &13C) spectral studies all the mononuclear derivatives have been obtained in tetrahedr… Show more
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