The field of sensor applications has witnessed substantial growth in diverse domains, including agriculture, food, oil, environment, and medicine. Among the varied methodologies employed, electrochemical methods stand out. The judicious selection of appropriate materials in this context significantly augments sensor efficiency. Zeolitic Imidazolate Framework 67 (ZIF 67), a highly porous material with an expansive surface area, offers facile synthesis, yet is impeded by limited conductivity. The introduction of additional metal derivatives has been reported to enhance its conductivity, with manganese, a transition metal, identified for its potential conductivity improvement and its influence on particle size. Thus, this paper aims to comprehensively explore the properties of manganese-modified ZIF 67, spanning structural, morphological, and electrochemical properties. Research findings indicate that manganese doping enhances crystallinity, as evident from X-ray diffraction analysis, while also impacting particle size (from
x
¯
514.4 nm to 944 nm), as assessed through SEM measurements. Furthermore, electrochemical performance reveals heightened peak current during redox processes reaching ±64 µA, indicative of improved conductivity from the ZIF 67 (±13 µA) and the bare (±43 µA). In light of these outcomes, this material emerges as a promising candidate for electrochemical sensor development.