The acoustic emission (AE) has been measured during the thermal cycling of
YBa2Cu3O7−X
ceramic samples through the 77–200 K temperature range at a rate of about
0.7 K s−1. AE signals have been detected in the vicinity of 100–168 K. It has been established
that the AE count rate exponentially increases and attains maxima at the
third cycle and then exponentially decreases. In contrast, the AE temperature
(TAE) is equal to 113 K at the first cycle and then decreases to minima at 100 K
at the third cycle and then increases again up to 168 K at the seventh
cycle. In suggesting a thermal activation process, both activation energies
E1−3 = 0.016 eV during 1–3
cycles and E3−7 = 0.032 eV during 3–7 cycles have been calculated. Based on the calculated
E value the equivalent
thermal loading σl = 133.12 kPa (Fl = 3.3 N) has been
calculated as well. This Fl
is more than two orders of magnitude greater than the yield stress value for
YBa2Cu3O7−X, so measured AE signals are due to arise from dislocations under thermal
stresses. The behaviour of AE on 1–3 cycles is explained as both an annihilation
between postsintering dislocations and dislocations arising due to anisotropic
thermal expansion of the crystallographic lattice as well as the appearance of
work hardening caused by the dislocations arising due to anisotropic thermal
expansion of the crystallographic lattice on 3–7 cycles only, whereas the behaviour of
TAE
is explained as the appearance of the ‘thermal’ Kaiser’s effect during the thermal cycling.