Accelerated solvent extraction-gel permeation chromatography-gas chromatography-tandem mass spectrometry to rapid detection of clotrimazole residue in animal-derived food

Han, Chao; Hu, Beizhen; Jin, Na; Jin, Jianchang; Yu, Zuolong; Huang, Chaoqun; Shen, Yan

doi:10.1016/j.lwt.2021.111248

Cited by 12 publications

(4 citation statements)

References 31 publications

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“…This method is fast, accurate, and highly sensitive. Han et al [27] combined accelerated solvent extraction with gel permeation chromatography to detect clotrimazole residues in beef and bovine kidney. Yu et al [28] developed an accelerated solvent extraction method for extracting seven tetracycline compounds from beef and liver, and the trichloroacetic acid/acetonitrile was extracted at a temperature of 60 • C and a pressure of 65 bar.…”

Section: Accelerated Solvent Extractionmentioning

confidence: 99%

A Review of Veterinary Drug Residue Detection: Recent Advancements, Challenges, and Future Directions

Jun

Wan

2023

Sustainability

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Veterinary drug residues of common food (milk, meat) have posed serious threats to the environment and human health, making the quality and safety of agricultural, livestock, and aquatic products increasingly prominent. With the widespread use of veterinary drugs and the requirements for food safety, it has become urgent to detect veterinary drug residues in animal-derived foods. So far, few studies have systematically reviewed the progresses, challenges, and future directions in veterinary drug residue detection. A thorough review on the current advancements, challenges, and potential future directions of veterinary drug residue detection will be extremely beneficial and timely. This study reviewed recent developments of detection technology of veterinary drug residues. The current issues and challenges in veterinary drug residue detection were examined and highlighted. Finally, future proposals on directions and prospects for veterinary drug residue detection were suggested. High-throughput and high-sensitivity veterinary drug detection technology, sample pretreatment technology for rapid processing, and the fusion of multiple detection methods were recommended as the main directions for the future development of veterinary drug residue detection. It was suggested to develop the analysis and detection technologies of veterinary drug residue towards high automation, high sensitivity, and high throughput in the future. This review provides new ideas and strategies for the rapid development of animal husbandry industry and protecting consumers’ physical health and food safety.

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Section: Accelerated Solvent Extractionmentioning

confidence: 99%

A Review of Veterinary Drug Residue Detection: Recent Advancements, Challenges, and Future Directions

Jun

Wan

2023

Sustainability

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“…The extraction and cleanup processes are also critical steps in increasing the overall speed and sensitivity of the detection. Currently, there are many pretreatment methods for detecting pesticide residues, for instance, solid-phase extraction, , liquid–liquid extraction, and gel permeation chromatography. , These methods demand special equipment, large amounts of solvents, complicated pretreatment steps, and high costs, which limit the rapid detection of pesticide trace analysis in TCM. Anastassiades et al established the QuEChERS method in 2003 .…”

Section: Introductionmentioning

confidence: 99%

Simultaneous Determination of 26 Pesticide Residues in Traditional Chinese Medicinal Leeches by Modified QuEChERS Coupled with HPLC–MS/MS

Zhou

Huang

et al. 2023

ACS Omega

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A Quick, Easy, Cheap, Effective, Rugged, and Safe (QuEChERS) pretreatment technique combined with HPLC–MS/MS was established to detect 26 pesticides in traditional Chinese medicinal leeches. The sample was extracted by acetonitrile solution with sodium acetate-0.1% (v/v) acetic acid as a buffer system, then cleaned up by a mixture of 750 mg of MgSO4, 150 mg of C18, and 150 mg of PSA, separated by an ACQUITY BEH C18 column, and determined in the dynamic multiple reaction mode. Under the optimized conditions, the peak areas of the 26 pesticides in leeches showed good linearity (r > 0.99) between their mass concentrations from 1 to 100 μg/L. At the spike levels of 10, 20, and 100 μg/kg, the recoveries of 26 pesticides in leeches were 72.9–101.6% with an RSD of 1.1–12.8%, an LOQ of 10 μg/kg, and an LOD of 0.1–5.4 μg/kg. This method is easy, rapid, sensitive, and practical and meets the requirements of pesticide residue detection standards.

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“…These challenges suggest the importance of improving food analysis methods and detection techniques for monitoring food contamination. Over the past decades, various analytical methods have been developed for qualitative/quantitative food analysis [ 13 , 14 , 15 , 16 ]. On account of their fast analysis speed, simplicity, low cost, inexpensive equipment, and no background interference, ECL-based biosensors are attracting increasing attention in food analysis.…”

Section: Introductionmentioning

confidence: 99%

Nanomaterials-Based Electrochemiluminescence Biosensors for Food Analysis: Recent Developments and Future Directions

Zhou

Jia

et al. 2022

Biosensors

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Developing robust and sensitive food safety detection methods is important for human health. Electrochemiluminescence (ECL) is a powerful analytical technique for complete separation of input source (electricity) and output signal (light), thereby significantly reducing background ECL signal. ECL biosensors have attracted considerable attention owing to their high sensitivity and wide dynamic range in food safety detection. In this review, we introduce the principles of ECL biosensors and common ECL luminophores, as well as the latest applications of ECL biosensors in food analysis. Further, novel nanomaterial assembly strategies have been progressively incorporated into the design of ECL biosensors, and by demonstrating some representative works, we summarize the development status of ECL biosensors in detection of mycotoxins, heavy metal ions, antibiotics, pesticide residues, foodborne pathogens, and other illegal additives. Finally, the current challenges faced by ECL biosensors are outlined and the future directions for advancing ECL research are presented.

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Accelerated solvent extraction-gel permeation chromatography-gas chromatography-tandem mass spectrometry to rapid detection of clotrimazole residue in animal-derived food

Cited by 12 publications

References 31 publications

A Review of Veterinary Drug Residue Detection: Recent Advancements, Challenges, and Future Directions

A Review of Veterinary Drug Residue Detection: Recent Advancements, Challenges, and Future Directions

Simultaneous Determination of 26 Pesticide Residues in Traditional Chinese Medicinal Leeches by Modified QuEChERS Coupled with HPLC–MS/MS

Nanomaterials-Based Electrochemiluminescence Biosensors for Food Analysis: Recent Developments and Future Directions

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