Accelerated nitroxide-mediated polymerization of styrene and butyl acrylate initiated by BlocBuilder MA using flow reactors

Takabayashi, Ryo; Feser, Stephan; Yonehara, Hiroshi; Ryu, Ilhyong; Fukuyama, Takahide

doi:10.1039/d3py00709j

Polym. Chem.

2023

DOI: 10.1039/d3py00709j

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Accelerated nitroxide-mediated polymerization of styrene and butyl acrylate initiated by BlocBuilder MA using flow reactors

Ryo Takabayashi,

Stephan Feser,

Hiroshi Yonehara

et al.

Abstract: The nitroxide-mediated radical polymerization (NMP) of styrene (St) and butyl acrylate (BA) using BlocBuider MA under continuous flow reaction conditions showed higher conversion and smaller polydispersity index (Ð) values compared...

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2024

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Cited by 2 publications

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Recent advances on photochroms used as visible light photoinitiators of polymerization

Dumur

2024

European Polymer Journal

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Recent advances on photochroms used as visible light photoinitiators of polymerization

Dumur

2024

European Polymer Journal

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Efficient Flow Synthesis of Glycidyl Ether Using BuSnCl3 as a Mild Lewis Acid

Fukuyama,

Kasakado,

Nakamura

et al. 2024

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A ring-opening protocol of epichlorohydrin (2) with 2-ethylhexanol (1a) was investigated for the synthesis of chlorohydrin 3a. BuSnCl3 proved to be an efficient mild Lewis acid catalyst, yielding 3a with high selectivity. A scalable flow synthesis of 3a was successfully achieved by modifying the flow setup for scaling up. The flow synthesis of glycidyl ether 4a from 3a was also carried out in an efficient manner by using the basic treatment.

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Accelerated nitroxide-mediated polymerization of styrene and butyl acrylate initiated by BlocBuilder MA using flow reactors

Abstract: The nitroxide-mediated radical polymerization (NMP) of styrene (St) and butyl acrylate (BA) using BlocBuider MA under continuous flow reaction conditions showed higher conversion and smaller polydispersity index (Ð) values compared...

Cited by 2 publications

References 34 publications

Recent advances on photochroms used as visible light photoinitiators of polymerization

Recent advances on photochroms used as visible light photoinitiators of polymerization

Efficient Flow Synthesis of Glycidyl Ether Using BuSnCl3 as a Mild Lewis Acid

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