Eur. J. Chem. volume 5, issue 3, P497-502 2014 DOI: 10.5155/eurjchem.5.3.497-502.1080
Ola Ahmed Saleh, Aida Abd El-Sattar El-Azzouny, Hassan Youssef Aboul-Enein, Amr Mohamed Badawey
Abstract:

A comparative and stability-indicating reversed phase high performance liquid chromatographic study have been developed and validated for sitagliptin phosphate. The liquid chromatographic determination was achieved isocratically on Poroshell 120 EC-C18 (100 × 4.6 mm, i.d.; particle size, 2.7 µm), Pursuit 5PFP (150 × 4.6 mm, i.d.; particle size, 5 µm) and Chromolith performance RP-18e (100 × 4.6 mm, i.d.; macropore diameter, 2 µm) columns using a mobile phase consisting of methanol:water:triethylamine:acet…

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