A Time-Saving Approach to Parameter Studies in Microwave-Assisted Freeze Drying

Abstract

Microwave-assisted freeze drying (MFD) is particularly suited for drying heat-sensitive materials. However, optimizing process parameters is time-consuming due to lengthy individual experiments. This study investigates the feasibility of partial MFD for parameter studies, with the process being terminated after removing 20 wt% of the water contained. The proposed approach reduces the time required for parameter evaluation by 92.0% compared to complete MFD. It also enables the evaluation of the samples’ drying homogeneity. A subsequent parameter study based on partial MFD was then conducted to evaluate the effects of chamber pressure, microwave power, and microwave frequencies on the drying kinetics and drying homogeneity. Lowering the average chamber pressure from 0.87 mbar to 0.19 mbar reduced the process duration by 18.8%. An increase in the dissipated specific microwave power from 0.048 W/g to 0.143 W/g reduced the duration by 46.7%. The targeted application of frequencies increased the average energy efficiency to as high as 92.4%, contributing to a shortened process duration of up to 51.2%. Only the application of multiple frequencies caused a notable increase in drying homogeneity. In summary, this study demonstrates the feasibility and time-saving benefits of partial drying for parameter studies in MFD and potentially different types of drying processes.

Shrinkage properties of porous materials during drying: a review

“…In order to improve the drying efficiency and quality of porous materials, hybrid drying technology has been widely used in the drying of porous materials (Menon et al, 2020;Hii et al, 2021). Hybrid drying techniques for porous materials include hot air-vacuum drying (Zhao et al, 2014), freezing-microwave drying (Sickert et al, 2023), supercritical-hot air drying (Siddiqui et al, 2023), vacuum-microwave drying (González-Cavieres et al, 2021 and freezing-supercritical drying (Wang et al, 2019). By combining different drying methods, these techniques aim to achieve a more efficient and gentle drying process.…”