A solid-spiking matrix matched calibration strategy for simultaneous determination of cadmium and chromium in sediments by isotope dilution laser ablation inductively coupled plasma mass spectrometry

Terán-Baamonde, J.; Carlosena, A.; Soto-Ferreiro, R. M.; Andrade, Javier; Cantarero-Roldán, Alicia M.; Muniategui-Lorenzo, Soledad

doi:10.1039/c9ja00335e

Cited by 3 publications

(1 citation statement)

References 35 publications

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“…Due to a lack of certified reference materials with the same matrix compound, the method of standard additions (addition calibration) was chosen to calibrate the spectrometer. This approach is considered as successful when using laser ablation with ICP-MS [29,30].…”

Section: Resultsmentioning

confidence: 99%

Determination of Boron, Lithium and Some Metals in Fly Ash by Laser Ablation ‒ Inductively Coupled Plasma ‒ Optical Emission Spectr ometry

Kolmykov

2022

Eurasian Chem. Tech. J.

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To avoid potentially harmful wet sample preparation is offered to use laser ablation (LA) ‒ inductively coupled plasma ‒ optical emission spectrometry (ICP-OES) as a method for the elemental analysis of fly ash for boron, lithium, and some metals. For this purpose, synthetic samples were prepared by spiking with dissolved standards. As a result, great stability of calibration curves was achieved. It was found that a particle diameter less than 80 μm in fly ash is enough to have a satisfying homogeneity for successful calibration in the method of standard additions. The average recovery test for reference materials used in the study was 16–77% of the certified values for the elements observed. The low results might be the effect of spiking with calibration samples in the liquid state. This type of analysis requires further investigation. According to the results of elemental analysis, the content of boron and lithium was determined for ZUK-2 and SO-1, which was not previously noticed in other papers.

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Section: Resultsmentioning

confidence: 99%

Determination of Boron, Lithium and Some Metals in Fly Ash by Laser Ablation ‒ Inductively Coupled Plasma ‒ Optical Emission Spectr ometry

Kolmykov

2022

Eurasian Chem. Tech. J.

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Flame atomic absorption spectrometric determination of total chromium and cadmium in bean samples after ultrasonic-assisted microextraction using ionic liquid Aliquat-336

et al. 2020

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Calibration approaches in laser ablation inductively coupled plasma mass spectrometry for bioimaging applications

Mervič,

Šala,

Theiner

2024

TrAC Trends in Analytical Chemistry

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A solid-spiking matrix matched calibration strategy for simultaneous determination of cadmium and chromium in sediments by isotope dilution laser ablation inductively coupled plasma mass spectrometry

Abstract: New quantification of Cd and Cr in sediments by isotope dilution LA-ICPMS, significantly simplifies and shortens the isotope dilution step.

Cited by 3 publications

References 35 publications

Determination of Boron, Lithium and Some Metals in Fly Ash by Laser Ablation ‒ Inductively Coupled Plasma ‒ Optical Emission Spectr ometry

Determination of Boron, Lithium and Some Metals in Fly Ash by Laser Ablation ‒ Inductively Coupled Plasma ‒ Optical Emission Spectr ometry

Flame atomic absorption spectrometric determination of total chromium and cadmium in bean samples after ultrasonic-assisted microextraction using ionic liquid Aliquat-336

Calibration approaches in laser ablation inductively coupled plasma mass spectrometry for bioimaging applications

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