“…1 With the discovery of many excellent physical and chemical properties such as high electrical conductivity, abundant surface groups, tunable band gap, high specific surface area, and hydrophilicity, it has great potential for applications in energy storage, catalysis, optoelectronics, and separation. 2–5 In general, MXene can be obtained by etching the MAX phase, which can be expressed as M n +1 AX n ( n = 1, 2 or 3), where “M” denotes the transition metals of the first few groups, “A” refers to a main group element ( e.g. , Al, Si, or Ga), and “X” refers to C or N. 6 So far, F-containing solution etching is the most classical preparation method with appreciable reproducibility and steady preparation of single-layer MXene sheets, which clears the obstacles for research work in this direction.…”