volume 6, issue 67, P62656-62667 2016
DOI: 10.1039/c6ra09695f
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Abstract: We present a novel approach to the solid-state synthesis of garnet-type cubic Li7La3Zr2O12 (c-LLZO) nanostructured particles with 1.0 mass% Al at 750 o C within 3 h. In contrast to conventional solid-state processes, a highly reactive precursor was prepared in two steps: (i) by homogenizing the stoichiometric mixture without Li, and (ii) subsequent addition of Li in the form of an ethanolic solution of lithium acetate. The actual composition determined by ICP analysis was Li6.61La3Zr2Al0.13O11.98. Sintering …

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