Abstract:Abstract.2,10-Ethano-10-norandrost-4-ene-3,17-dione, C2oH2602, Mr= 298.43, orthorhombic, P2~2121, a--7-566 (3), b= 11.478 (7), c= 18.681 (7)A, V= 1622.5(13)A 3, Z=4, D m (flotation in aqueous ZnC12) --1.21 (2), D x = 1.222 Mg m -3, 2(Mo Ka--) = 0.71073 A, #= 0.0716 mm -1, F(000) = 648, T= 293 K, R --0.038, wR -0.052 for 1629 observations. The title molecule was prepared as part of synthetic efforts in the design of inhibitors for steroid 5a-reductase. Based upon a desire to lift the A ring in the fl direction,… Show more
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