A novel approach for isolation of essential oil from fresh leaves of Magnolia sieboldii using microwave-assisted simultaneous distillation and extraction

Chen, Fengli; Zu, Yuangang; Yang, Lei

doi:10.1016/j.seppur.2015.09.066

Cited by 49 publications

(22 citation statements)

References 28 publications

(32 reference statements)

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“…In contrast, the use of dichloromethane as the extraction solvent gave much higher yields. The results are consistent with the reference [31]. Based on these results, dichloromethane was identified as the optimum solvent for the extraction of the essential oil from T. chinensis var.…”

Section: Effect Of Extraction Solvent On the Yield Of Essential Oilsupporting

confidence: 88%

A Microwave-Assisted Simultaneous Distillation and Extraction Method for the Separation of Polysaccharides and Essential Oil from the Leaves of Taxus chinensis Var. mairei

Zhao

et al. 2016

Applied Sciences

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An efficient microwave-assisted simultaneous distillation and extraction (MA-SDE) method has been developed for the separation of polysaccharides and essential oil from Taxus chinensis var. mairei. The key operating parameters for MA-SDE were optimized by single factor and central composite design experiments, and the optimal conditions were found to include a particle size of 60-80 mesh, liquid/solid ratio of 22.5 mL/g, extraction time of 17.5 min, microwave power of 547 W, and dichloromethane was used as the extraction solvent of the essential oil. The yields obtained for polysaccharides and essential oil under the optimized conditions were 6.39%˘0.12% and 0.27%˘0.03%, respectively. The MA-SDE method was also compared with conventional heat reflux extraction (HRE) and hydrodistillation extraction (HDE). The MA-SDE method not only allowed for the simultaneous extraction of polysaccharides and essential oil, but also completed the task with a much shorter extraction time of 17.5 min (HRE and HDE required 3 and 6 h, respectively). Furthermore, the MA-SDE method gave increased extraction yields for polysaccharides (1.14-fold higher than HRE) and essential oil (1.23-fold higher than HDE). Based on these results, this MA-SDE method represents a rapid and efficient technique for the simultaneous extraction of polysaccharides and essential oil.

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Section: Effect Of Extraction Solvent On the Yield Of Essential Oilsupporting

confidence: 88%

A Microwave-Assisted Simultaneous Distillation and Extraction Method for the Separation of Polysaccharides and Essential Oil from the Leaves of Taxus chinensis Var. mairei

Zhao

et al. 2016

Applied Sciences

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“…The coefficient of variation (CV) is often used to determine the reproducibility of the model [50]: the greater the CV, the higher the variation of the mean value [51]. The low coefficient of variation of 1.84% implied a high degree of precision and reliability of the experiments conducted.…”

Section: /33mentioning

confidence: 99%

A new approach for obtaining trans-resveratrol from tree peony seed oil extracted residues using ionic liquid-based enzymatic hydrolysis in situ extraction

Chen

Zhang²,

et al. 2016

Separation and Purification Technology

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“…The conventional extraction methods for analyzing volatile food substances are vacuum simultaneous steam distillation solvent extraction (V-SED) [ 11 , 12 ], direct solvent extraction (DSE) [ 13 , 14 ], solvent-assisted flavor evaporation (SAFE) [ 15 ], and steam distillation under reduced pressure (DRP-LLE) [ 16 , 17 ]. However, these methods need large amounts of extraction solvents, have low recovery, and can be used only with low-fat samples.…”

Section: Introductionmentioning

confidence: 99%

Analysis of Volatile Compounds in Soju, a Korean Distilled Spirit, by SPME-Arrow-GC/MS

Cha

Chin

Lee

et al. 2020

Foods

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The SPME Arrow technology—a novel solid phase micro-extraction technique—was used to analyze Soju, a traditional Korean distilled liquor, in barrels made of Quercus spp. The volatile compounds detected when the barrels were toasted were analyzed. Five types of sorbents—carbon wide range/polydimethylsiloxane, divinylbenzene/carbon wide range/polydimethylsiloxane, divinylbenzene/polydimethylsiloxane, polydimethylsiloxane, and polyacrylate—were used for this investigation. Fifty-four volatile compounds were detected in Soju using gas chromatography/mass spectrometry. A high extraction efficiency was obtained using carbon wide range/polydimethylsiloxane. Nineteen samples were analyzed using barrels made of six species of carbonated oak (Q. aliena, Q. variabilis, Q. dentate, Q. acutissima, Q. mongolica, and Q. serrata) and control groups in three ways: noncharring, medium charring, and heavy charring. Ethanol, 1-propanol, isoamyl acetate, and isoamyl alcohol can be used as indicator volatile components for Soju and other such traditional Korean distilled liquors. We believe our study results can be used to design better analysis methods for Soju and other distilled liquors.

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A novel approach for isolation of essential oil from fresh leaves of Magnolia sieboldii using microwave-assisted simultaneous distillation and extraction

Cited by 49 publications

References 28 publications

A Microwave-Assisted Simultaneous Distillation and Extraction Method for the Separation of Polysaccharides and Essential Oil from the Leaves of Taxus chinensis Var. mairei

A Microwave-Assisted Simultaneous Distillation and Extraction Method for the Separation of Polysaccharides and Essential Oil from the Leaves of Taxus chinensis Var. mairei

A new approach for obtaining trans-resveratrol from tree peony seed oil extracted residues using ionic liquid-based enzymatic hydrolysis in situ extraction

Analysis of Volatile Compounds in Soju, a Korean Distilled Spirit, by SPME-Arrow-GC/MS

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