This work describes a semester-long
learning module designed to
equip students with the analytical and practical skills necessary
to be successful in an interdisciplinary polymer research environment.
This learning module combines laboratory experiments involving both
synthesis and materials characterization with lectures in polymer
theory, and encourages chemists and engineers to learn alongside one
another. Specifically, students learn air-free Schlenk technique to
facilitate the atom transfer radical polymerization (ATRP) of a series
of homo- and copolymers made from n-butyl methacrylate
(BMA) and methyl methacrylate (MMA) monomers. Students analyze these
polymers using techniques that traverse the interdisciplinary spectrumincluding
Gel Permeation Chromatography (GPC), Proton-Nuclear Magnetic Resonance
(1H NMR) spectroscopy, Thermogravimetric Analysis (TGA),
Differential Scanning Calorimetry (DSC), and Dynamic Mechanical Analysis
(DMA)and learn about the theory and mathematics behind the
measurements. Ultimately, this hands-on experience in polymer material
design bridges the structure–property relationships taught
by classical and applied polymer theory.