1990
DOI: 10.1111/j.1365-2621.1990.tb06078.x
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A Method for the Rapid Analysis of Headspace Volatiles of Raw and Roasted Peanuts

Abstract: A rapid headspace analysis method for evaluating the flavor quality of peanuts using gas chromatography has been developed and Lested. Samples are ground. heated in glass vials for 30 min at 150°C. and the deadspaceinjectkd using a gas tight syringe. After initial startup, one can screen samples for flavor defects at the rate of four per hour. Of the peaks produced from peanut headspace analysis, most have been identified by gas chromatography/mass spectrometty and eight have been related to specific flavor ch… Show more

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Cited by 49 publications
(50 citation statements)
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“…In addition, several smaller peaks representing abusive drying (ethanol), fruity flavor (2-methyl propanal), degree of roast (2-butanone), aging (2-and 3-methyl butanal), tongue or throat bum (pentanal), and beany flavor (hexanal) (Young and Hovis 1990) were also detected in the headspace gases.…”
Section: Resultsmentioning
confidence: 97%
“…In addition, several smaller peaks representing abusive drying (ethanol), fruity flavor (2-methyl propanal), degree of roast (2-butanone), aging (2-and 3-methyl butanal), tongue or throat bum (pentanal), and beany flavor (hexanal) (Young and Hovis 1990) were also detected in the headspace gases.…”
Section: Resultsmentioning
confidence: 97%
“…A selected ion mode (SIM) method was developed using H 3 O + , NO + , or O 2 + as precursor ions; refer to Smith and Spanel () for more information on SIFT‐MS. The method developed was based on known volatiles present in raw and roasted peanuts (Shu and Waller ; Brown and others ; Buckholz and Daun ; Pattee and Singleton ; Young and Hovis ; Singleton and Pattee ; Coleman and others ; Braddock and others ; Ku and others ; Matsui and others ; Smyth and others ; Mexis and Kontominas ). Volatile kinetics are shown in Table .…”
Section: Methodsmentioning
confidence: 99%
“…Following heating of tissue (1.5g) in a 5ml conical vial for 15 min at 90°C headspace (1.5ml) was removed with a gas-tight syringe and subjected to the chromatographic conditions described by Young & Hovis (1990). Each sample was analysed in triplicate.…”
Section: Headspace Volatile Analysesmentioning
confidence: 99%