2017
DOI: 10.1039/c6gc02888h
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A laboratory-scale annular continuous flow reactor for UV photochemistry using excimer lamps for discrete wavelength excitation and its use in a wavelength study of a photodecarboxlyative cyclisation

Abstract: A novel annular flow reactor for UV photochemistry.

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Cited by 27 publications
(23 citation statements)
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References 65 publications
(82 reference statements)
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“…As with thermal reactors, options for photochemical reactors have bifurcated into home-built and commercial platforms, essentially light-transparent chips or coil reactors. [89][90][91] Photochemistry's true niche is the formation of synthetically inaccessible molecules. Challenging through standard chemical transformations, the utilization of Scheme 1 Telescoped scheme for the continuous flow production of Ciprofloxacin.…”
Section: Reactor Selectionmentioning
confidence: 99%
“…As with thermal reactors, options for photochemical reactors have bifurcated into home-built and commercial platforms, essentially light-transparent chips or coil reactors. [89][90][91] Photochemistry's true niche is the formation of synthetically inaccessible molecules. Challenging through standard chemical transformations, the utilization of Scheme 1 Telescoped scheme for the continuous flow production of Ciprofloxacin.…”
Section: Reactor Selectionmentioning
confidence: 99%
“…In the first example DeLaney et al . describe an annular continuous flow reactor combined with a set of excimer lamp light sources for the irradiation with defined wavelengths (KrCl: 222 nm; XeBr: 282 nm; XeCl: 308) . The reactor itself consists of a stainless steel cooling finger (o.d.…”
Section: Reactor Concepts For Flow Photochemistrymentioning
confidence: 99%
“… Photodecarboxylative cyclisation of potassium N ‐phthalimido‐butanoate 6 with UV light in continuous flow …”
Section: Reactor Concepts For Flow Photochemistrymentioning
confidence: 99%
“…50 mL) was placed between the second and third reactor module to remove excess of acid after the dehydration step. A similar approach was described by DeLaney et al for the removal of base [21]. Heating was achieved in the third step by submerging the capillary coil in a water bath.…”
Section: Flow Reactor Designmentioning
confidence: 99%