“…Electrochemical sensors represent a capable advancement to complement the previously published procedures owing to their easy instrumentation, low cost, high selectivity and sensitivity, and signicant properties for the successful detection of heavy metal ions. [6][7][8][9][10][11][12][13][14] In this research, a simple, sensitive, and selective Pb 2+ sensor was developed based on (E)-N 0 -(benzo[d]dioxol-5-ylmethylene)-4-methyl-benzenesulfonohydrazide derivatives modied on a GCE with 5% conducting Naon polymer matrix via an electrochemical approach under ambient conditions. [1,3]-dioxole carbaldehyde, BSH, 4-MBSH, AgNO 3 , AuCl 3 , CaCl 2 , FeCl 3 , MgCl 2 , Pb(NO 3 ) 2 , ZnSO 4 , SnCl 2 , EtOH, NaH 2 PO 4 , Na 2 HPO 4 , and NF (5.0 weight% in water and lower aliphatic alcohol containing 45.0% water) were purchased from Sigma Aldrich Company, KSA and used as received.…”