A facile one-pot synthesis of new functionalized pyrazolone-1,4-dithiafulvene hybrids

Salehzadeh, Jaber; Nasiri, Farough

doi:10.1007/s11030-022-10473-x

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Synthesis and Characterization Of Products1

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2023

2024

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Cited by 5 publications

(1 citation statement)

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“…Although the mechanistic details of the reaction between pyrazolones 3 and carbon disul de in the presence of ECH are unknown, a possible explanation is proposed in Scheme 4. Initially, tautomeric intermediates I and II are generated from the reaction between pyrazolones 3 and carbon disul de in the presence of triethylamine [27,28]. Subsequently, the sulfur anion of I or II is added to ECH to generate intermediate III.…”

Section: Synthesis and Characterization Of Productsmentioning

confidence: 99%

Facile one-pot synthesis of hydroxylated 1,3-dithiane-pyrazolone hybrids

Rabiei,

Nasiri

2024

Res Chem Intermed

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This study presents an effective one-pot strategy for the synthesis of hydroxylated 1,3-dithianepyrazolone hybrids. The process involves a reaction between pyrazolone derivatives and carbon disul de in the presence of epichlorohydrin (ECH). The structural elucidation of the products was accomplished using various spectroscopic techniques. To further corroborate the proposed reaction mechanism, enantiomerically pure ECH was utilized.

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Section: Synthesis and Characterization Of Productsmentioning

confidence: 99%