2023
DOI: 10.1016/j.mencom.2023.02.003
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A convenient synthesis of N,N',N''-trisubstituted diethylenetriamines

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Cited by 2 publications
(2 citation statements)
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“…At first, diethylenetriamine pro-ligands 1a – 8a were synthesized by a reported method . New aluminum complexes 5 – 8 were synthesized with 58–74% yields by reacting a solution of diethylenetriamine pro-ligands 5a – 8a with a commercially available 2 M solution of AlMe 3 in toluene (Scheme ).…”
Section: Resultsmentioning
confidence: 99%
See 1 more Smart Citation
“…At first, diethylenetriamine pro-ligands 1a – 8a were synthesized by a reported method . New aluminum complexes 5 – 8 were synthesized with 58–74% yields by reacting a solution of diethylenetriamine pro-ligands 5a – 8a with a commercially available 2 M solution of AlMe 3 in toluene (Scheme ).…”
Section: Resultsmentioning
confidence: 99%
“…L -LA was recrystallized from toluene and sublimed in vacuo , and ε-CL was distilled over CaH 2 . Pro-ligands ( 1a - 8a ) and 2-(benzyloxycarbonyl)-2-methyltrimethylene carbonate were synthesized according to the literature procedures.…”
Section: Methodsmentioning
confidence: 99%