2006
DOI: 10.1016/j.matchar.2005.11.005
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A complex procedure for describing porosity in precision cast elements of aircraft engines made of MAR-M 247 and MAR-M 509 superalloys

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Cited by 22 publications
(10 citation statements)
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“…The determination of gas and shrinkage porosity was carried out on the polished samples by quantitative metallography. The complex procedure of the quantitative evaluation of gas and shrinkage porosity, described in [8], was used. The samples were mechanically ground on abrasive paper (grit sizes: 320, 600, 800 and 1000), polished with diamond suspensions (grit sizes: 9 μm, 3 μm, 1 μm and 0.25 μm, respectively) and with alumina suspension (grit size: 0.05 μm).…”
Section: Methodsmentioning
confidence: 99%
“…The determination of gas and shrinkage porosity was carried out on the polished samples by quantitative metallography. The complex procedure of the quantitative evaluation of gas and shrinkage porosity, described in [8], was used. The samples were mechanically ground on abrasive paper (grit sizes: 320, 600, 800 and 1000), polished with diamond suspensions (grit sizes: 9 μm, 3 μm, 1 μm and 0.25 μm, respectively) and with alumina suspension (grit size: 0.05 μm).…”
Section: Methodsmentioning
confidence: 99%
“…For microstructural characterization, the samples were sectioned from the mid-airfoil areas, perpendicular to the blade axis. The samples were prepared according to procedure described earlier [9][10][11]. After ultrasonic cleaning, electrochemical etching in 10% oxalic acid solution (voltage: 6V, time: 5s) was applied.…”
Section: Methodsmentioning
confidence: 99%
“…For EBSD analysis, samples were additionally polished using an alumina suspension (grit size: 0.05 µm) for 5 h with vibration. The determination of internal porosity was carried out on polished samples by image analysis based on optical micrographs (using an Olympus GX-70 light microscope) in accordance with procedures described in literature [9][10][11].…”
Section: Methodsmentioning
confidence: 99%
“…Each section was measured in 10 places with 2.94 mm 2 analysis area. MetIlo software was used to calculate porosity values [8]. Average and maximum value (for the worst field) of the area fraction of pores A A of each cross-section have been noted.…”
Section: Experimental Methodsmentioning
confidence: 99%