Conducting polymers are critically important materials
in organic
electronic platforms relevant to sustainability (organic photovoltaics
and organic light-emitting diodes) and wearable electronics (organic
electrochemical transistors). However, most chemistry students do
not receive formal training in the fundamental properties and extensive
characterization of these fascinating materials. Described here are
four scaffolded learning modules adapted from the primary literature
and designed to build the fundamental understanding and practical
skills necessary for productive contribution to emerging research
in the field of conducting polymers and conducting polymer modified
electrodes (CPMEs). These activities were performed by first-year
chemistry graduate students and have been used in the lab to orient
and equip new student researchers with the electrochemical, spectroscopic,
and spectroelectrochemical skillsets central to working in CPMEs.
First year master’s students and undergraduate student researchers
worked individually to complete data collection, analysis, and interpretation
over three 4 h periods with additional time for sample preparation
and imaging. Alternatively, one or more of these modules can be adapted
and performed by pairs or groups of three over two 4 h lab periods
as part of an undergraduate course such as instrumental analysis,
polymers, and macromolecules, or as a capstone experience; instructions
for these and other modifications are as described herein. If lab
equipment and/or available time are limiting factors, sufficient sample
data are provided for use as dry laboratories. Through completion
of these modules, student researchers learn how to build chemically
rational explanations for the electrochemical and spectroscopic signals,
to collectively examine data from multiple complementary characterization
techniques, and to extract enabling structure–property relationships,
all while coming to see themselves as researchers and members of a
worldwide scientific community.