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Дикусар, Е. А.; Nechai, N. I.; Поткин, В. И.; Kaberdin, R. V.; Козлов, Н. Г.; Ковганко, Н. В.

doi:10.1023/a:1024865931052

Chemistry of Natural Compounds

2003

DOI: 10.1023/a:1024865931052

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Е. А. Дикусар

N. I. Nechai

В. И. Поткин

et al.

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Cited by 2 publications

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“…The other esters IIb!IIm and IIIb!IIIg were prepared by reactions of Ia and Ib with alkanecarboxylic acid chlorides in the presence of pyridine [15,16]. To simplify the production process and improve the purity of the target products for their use in formulations for perfume and food industry, the esters were also prepared by the Schotten3Baumann reaction [9,17].…”

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Preparative Synthesis of Vanillin and Vanillal Alkanoates

et al. 2005

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Procedures for preparing vanillin and vanillal alkanoates were developed.Vanillin (4-hydroxy-3-methoxybenzaldehyde, Ia) and its homolog, vanillal (4-hydroxy-3-ethoxybenzaldehyde, Ib) are widely used in food and perfume industries [133]. Vanillin can also be used as a synthetic precursor of biologically active substances [4,5]. However, new processes in food industry demand new aroma chemicals that would have vanilla smell but be more heat-resistant than vanillin and stable in a wide range of pH in the presence of enzymes. These requirements stimulate chemists to prepare new vanillin and vanillal derivatives; many of them appeared to exhibit stronger vanilla smell, compared to the initial compounds, with diverse tints.Here we report convenient synthetic routes to vanillin (IIa!IIm) and vanillal (IIIa!IIIg) esters. 2 j RO g g CHO OC(O)RÌ I a3m, III a3g 2 j RO g g CHO OC(O)RÌ I a3m, III a3g

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Preparative Synthesis of Vanillin and Vanillal Alkanoates

et al. 2005

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Synthesis of Novel Vanillin Derivatives Containing Isothiazole Moieties and its Synergistic Effect in Mixtures with Insecticides

Поткин

Zubenko

Bykhovetz

et al. 2009

Natural Product Communications

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Cited by 2 publications

References 2 publications

Preparative Synthesis of Vanillin and Vanillal Alkanoates

Preparative Synthesis of Vanillin and Vanillal Alkanoates

Synthesis of Novel Vanillin Derivatives Containing Isothiazole Moieties and its Synergistic Effect in Mixtures with Insecticides

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