A method for production of calibration blocks on the basis of a homogeneous disperse weakly magnetic mixture of ferromagnetic and paramagnetic materials, as well as the methods for assessing their parameters, are developed. A set of calibration blocks with a magnetic susceptibility ranging from 5 × 10 -3 to 2.5 × 10 -2 SI units has been made. This set enables efficient calibration of the devices for measuring magnetic susceptibility. The efficiency of calculation methods is confirmed for the assessment of a calibration block's magnetic susceptibility. The calculated result coincides with the experimental value = 1.98 SI units with an error of 1%.INTRODUCTION As was shown in the first part of this study [1], calculation methods are only applicable for normalizing the limiting values of a disperse mixture's magnetic susceptibility and, in particular, the values close to 2 SI units, which are due to encasement of the mixture in a spherical shell made of a dielectric with a magnetic susceptibility of the material of ~ 10 -5 SI units. These calculations were used as a basis for making a calibration specimen that consists of a disperse ferromagnetic mixture made of grade 600 HH ferrite ( χ m > 400 SI units) encased in a spherical glass bulb and compressed to a volume concentration of C V ≅ 0.9, i.e., to 90%. The numerical value of the calibration specimen's magnetic susceptibility is = 1.99 SI units with an error of ± 1%. However, the obtained value of the calibration specimen's magnetic susceptibility cannot be directly used for calibrating devices for measuring magnetic susceptibility [2] within their working range 5 × 10 -3 -25 × 10 -3 SI units.The developed specimen can be used for calibrating purposes during the measurements of the magnetic susceptibility of materials in the vicinity of 2 SI units. It can also be used for certifying measurement methods or, as in this case, for calibrating measurement devices.Therefore, it is necessary to develop calibration blocks of magnetic susceptibility made of a weakly magnetic disperse mixture. Creation of such calibration blocks involves the solution of a number of problems of determining and producing the materials for the disperse mixture that are characterized by the required composition and high homogeneity; investigation of the mixture's magnetic properties; and selection of the material, the shape, and the dimensions of a nonmagnetic shell encasing the disperse mixture.