71Ga and 69Ga nuclear magnetic resonance study of β-Ga2O3: resolution of four- and six-fold coordinated Ga sites in static conditions

Massiot, Dominique; Farnan, Ian; Gautier, N.; Trumeau, Dominique; Trokiner, A.; Coutures, Jean-Pierre

doi:10.1016/0926-2040(95)00002-8

Cited by 314 publications

(376 citation statements)

References 14 publications

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“…To allow unambiguous simulation especially when multiple interactions are present, although distortions can be taken in account, collecting undistorted experimental spectra pays dividends. Using frequency offset techniques, such as VOCS, allow such spectra to be collected [26].…”

Section: Methods For Improving Sensitivity and Wideline Observation Fmentioning

confidence: 99%

Recent technique developments and applications of solid state NMR in characterising inorganic materials

Hanna

Smith

2010

Solid State Nuclear Magnetic Resonance

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A broad overview is given of some key recent developments in solid state NMR techniques that have driven enhanced applications to inorganic materials science. Reference is made to advances in hardware, pulse sequences and associated computational methods (e.g. first principles calculations, spectral simulation), along with their combination to provide more information about solid phases. The resulting methodology has allowed more nuclei to be observed and more structural information to be extracted. Cross referencing between experimental parameters and their calculation from the structure has seen an added dimension to NMR as a characterisation probe of materials. Emphasis is placed on the progress made in the last decade especially from those nuclei that were little studied previously. The general points about technique development and the increased range of nuclei observed are illustrated through a range of specific exemplars from inorganic materials science.

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Section: Methods For Improving Sensitivity and Wideline Observation Fmentioning

confidence: 99%

Recent technique developments and applications of solid state NMR in characterising inorganic materials

Hanna

Smith

2010

Solid State Nuclear Magnetic Resonance

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“…Smith has summarized the experimental approaches for observing low-frequency nuclei such as 35/37 Cl. 7 A so-called 'whole-echo' acquisition has also been applied, 145,146 which increases the signal-to-noise by 2 1/2 .…”

Section: Powdered Samplesmentioning

confidence: 99%

Solid-state NMR spectroscopy of the quadrupolar halogens: chlorine-35/37, bromine-79/81, and iodine-127

Bryce

Sward

2006

Magn. Reson. Chem.

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“…In most cases, the NMR powder patterns were much wider than the excitation bandwidth achievable with a standard high power rectangular pulse; hence, spectra were acquired by stepping the transmitter frequency across the entire central transition (CT) powder pattern in even increments, collecting the individual subspectra, and coadding them to form the total pattern 41,42 (see the Supporting Information, Tables S1 and S2, for full experimental details). Barium chemical shifts were referenced toa1Maqueous solution of BaCl 2 (δ iso ) 0.0 ppm).…”

Section: Solid-state Nmrmentioning

confidence: 99%

Solid-State ¹³⁷Ba NMR Spectroscopy: An Experimental and Theoretical Investigation of ¹³⁷Ba Electric Field Gradient Tensors and Their Relation to Structure and Symmetry

Hamaed

Udachin

et al. 2010

J. Phys. Chem. B

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71Ga and 69Ga nuclear magnetic resonance study of β-Ga2O3: resolution of four- and six-fold coordinated Ga sites in static conditions

Cited by 314 publications

References 14 publications

Recent technique developments and applications of solid state NMR in characterising inorganic materials

Recent technique developments and applications of solid state NMR in characterising inorganic materials

Solid-state NMR spectroscopy of the quadrupolar halogens: chlorine-35/37, bromine-79/81, and iodine-127

Solid-State ¹³⁷Ba NMR Spectroscopy: An Experimental and Theoretical Investigation of ¹³⁷Ba Electric Field Gradient Tensors and Their Relation to Structure and Symmetry

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71Ga and 69Ga nuclear magnetic resonance study of β-Ga2O3: resolution of four- and six-fold coordinated Ga sites in static conditions

Cited by 314 publications

References 14 publications

Recent technique developments and applications of solid state NMR in characterising inorganic materials

Recent technique developments and applications of solid state NMR in characterising inorganic materials

Solid-state NMR spectroscopy of the quadrupolar halogens: chlorine-35/37, bromine-79/81, and iodine-127

Solid-State 137Ba NMR Spectroscopy: An Experimental and Theoretical Investigation of 137Ba Electric Field Gradient Tensors and Their Relation to Structure and Symmetry

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Solid-State ¹³⁷Ba NMR Spectroscopy: An Experimental and Theoretical Investigation of ¹³⁷Ba Electric Field Gradient Tensors and Their Relation to Structure and Symmetry