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利弘, 瀬尾; 琢也, 法元; 敏夫, 加倉井

doi:10.1246/nikkashi.1982.485

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1982

2017

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“…5, 167.4, 138.07, 136.6, 132.9, 128.9, 128.8, 125.6, 25.7, 21.5 176.3, 169.5, 167.4, 137.1, 135.4, 130.1, 129.1, 25.7 175.5, 170.1, 169.8, 165.9, 136.7, 136.5, 132.3, 132.2, 128.9, 128.5, 128.4, 31.4, 31.4, 29.2, 26.5, 26.5, 26.2, 25.6, 22.5, 14.4 271.1923, found 271.1925. 4-Ethyl-6-(p-tolyl)-1,3,5-triazin-2-amine (4f). 12 Eluent: petroleum ether/ethyl acetate (4:1). Yield 35.4 mg (55%).…”

Section: ■ Experimental Sectionmentioning

confidence: 99%

Base-Mediated Synthesis of Unsymmetrical 1,3,5-Triazin-2-amines via Three-Component Reaction of Imidates, Guanidines, and Amides or Aldehydes

et al. 2017

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A simple and efficient method for the base-mediated synthesis of unsymmetrical 1,3,5-triazin-2-amines has been developed. The protocol uses readily available imidates, guanidines, and amides or aldehydes as the starting materials, cesium carbonate as the base, no catalyst or additive is required, and the three-component reaction provides diverse 1,3,5-triazin-2-amines in moderate to good yields with tolerance of wide functional groups.

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Section: ■ Experimental Sectionmentioning

confidence: 99%