Oxygenated heterocyclic compounds to differentiate Citrus spp. essential oils through metabolomic strategies

Masson, Jerome; Liberto, Erica; Beolor, Jean Claude; Brevard, Hugues; Bicchi, Carlo; Rubiolo, Patrizia

doi:10.1016/j.foodchem.2016.03.057

Cited by 28 publications

(28 citation statements)

References 44 publications

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“…Until now, published HPTLC methods were limited to the analysis of a few furocoumarins whereas the 15 most commonly found in Citrus oils ( 1–15 ) can be analysed by HPLC‐DAD in 60 min and an additional 3 by UHPLC/TOF‐HRMS in 15 min …”

Section: Resultsmentioning

confidence: 99%

“…Two years later, Corbi et al developed a new RP‐HPLC‐high‐resolution/accurate MS method based on Orbitrap technology to quantify, in 40 min, seven furocoumarins with a linearity range of 0.01–1 mg kg −1 in an alcoholic perfume . Recently, Masson et al presented a 15‐min UHPLC/TOF‐HRMS method as a tool to characterize and discriminate authenticated commercial samples of Citrus essential oils . The method was used to quantify 18 furocoumarins and coumarins.…”

Section: Introductionmentioning

confidence: 99%

“…Highperformance liquid chromatography coupled with a diode array detector (HPLC-DAD) is the method of choice generally reported for their analysis. [15][16][17][18][19][20] In 2004, Frérot et al proposed a reversed phase HPLC method with UV detection at 310 nm to separate and quantify the 15 most common furocoumarins (1)(2)(3)(4)(5)(6)(7)(8)(9)(10)(11)(12)(13)(14)(15) in essential oils. 18 This method was validated in a collaborative ring test by the IFRA Analytical Working Group 8 years later.…”

mentioning

confidence: 99%

“…32,41 Recently, HPTLC with a scanning system has stimulated a growing interest for the routine determination of target compounds. 46 Thus, the aim of this study was (i) to propose a new HPTLC method to analyse the 20 most common furocoumarins (1)(2)(3)(4)(5)(6)(7)(8)(9)(10)(11)(12)(13)(14)(15)(16)(17)(18)(19)(20) found in perfumery raw materials for screening purposes ( Figure 1). and (ii) to propose a validated HPTLC method allowing the quantification of bergapten in essential oils in accordance with regulated limits.…”

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confidence: 99%

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HPTLC methods for qualitative and quantitative analysis of selected furocoumarins in essential oils

Borgne¹,

Cicchetti²,

Bertrand³

2017

Flavour & Fragrance J

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The concentration of furocoumarins, known to induce mutagenesis, carcinogenesis and photodermatitis under UV radiation, is limited by the EU cosmetic regulation in consumer products such as cosmetics, sun protection and bronzing formulations. The bergapten concentration is also limited by the International Fragrance Association. Analytical methods have been proposed for their quantification using high‐performance liquid chromatography (HPLC) coupled with UV detection or mass spectrometry with limits of detection (LOD) and quantification (LOQ) in accordance with the regulation. These methods are time and solvent consuming for routine quality control analyses. In this context, simple and fast HPLC methods in one‐ (1‐D) and two‐ (2‐D) dimensions were developed for the simultaneous analysis of the 15 most common furocoumarins reported in Citrus essential oils: psoralen, bergapten, xanthotoxin, isopimpinellin, oxypeucedanin, oxypeucedanin hydrate, byakangelicol, byakangelicin, heraclenin, 8‐geranyloxypsoralen, bergamottin, imperatorin, isoimperatorin, phellopterin, epoxybergamottin along with five other furocoumarins known to be present in Angelica, bergamot or Heracleum species: angelicin, bergaptol, isobergapten, psora‐4 and 5‐(4‐phenoxybutoxy)psoralen. The 1‐D method was validated for the quantification of bergapten using a Camag TLC Scanner as a detector. The LOD was determined at 2 mg/kg. The method was linear from 2 to 100 mg/kg and the method range was defined using accuracy profiles at with an 80% tolerance interval, with a 30% error, to be 5–100 mg/kg in acetonitrile and 13–100 mg/kg in matrix.

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Section: Resultsmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

mentioning

confidence: 99%

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confidence: 99%

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HPTLC methods for qualitative and quantitative analysis of selected furocoumarins in essential oils

Borgne¹,

Cicchetti²,

Bertrand³

2017

Flavour & Fragrance J

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“…Agricultural wastes from citrus fruit processing account for 50% of the total fruit weight (Cohn and Cohn, 1997). Most of these agricultural wastes are non-reusable, except a small portion that is used for the extraction of essential oils and the preparation of pectin and animal feeds (Malla et al, 2015;Liu et al, 2016;Masson et al, 2016). Hence, the effective use of citrus processing wastes is a research topic worthy of investigation.…”

Section: Introductionmentioning

confidence: 99%

Orange Peel Fiber and Tremella flava Fermented Powder Effectively Induce Exopolysaccharide Production by Lactobacillus plantarum SLC

Huang

Kao

et al. 2017

IJAB

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The aim of this study was to evaluate the effect of orange peel fiber powder (OPFP) in comparison to that of Tremella flava Chen fermented powder (TFP) on Lactobacillus plantarum SLC 13 exopolysaccharide (EPS) production. Growth of and EPS production by SLC 13 in MRS medium supplemented with different concentrations of glucose, OPFP, and TFP were investigated. The antioxidant activity of EPS and antibacterial property of the culture medium were investigated by adding 6% glucose, 2% OPFP, and 2% TFP to the SLC 13 culture medium. Supplementation with 6% glucose, 2% OPFP, and 2% TFP significantly promoted EPS production and bacterial viability. Maximum EPS production (2.6647 ± 0.0380 g/L) of SLC 13 was observed when 2% OPFP pretreated with 3 N HCl was added to the culture medium. Supplementation of 2% OPFP treated with 20 U xylanase, 20 U cellulase, and 10 U cellulase/10 U xylanase increased the EPS production by strain SLC 13. The highest reducing power and DPPH and ABTS radical scavenging activities of EPS were observed when the culture medium was supplemented with 6% glucose. Supplementation with 6% glucose and 2% OPFP enhanced the antibacterial property of the SLC 13 medium against Staphylococcus aureus and Salmonella typhimurium, respectively. Our findings that OPFP promotes growth, EPS production and antibacterial property of SLC 13 suggest that it has potential for industrial application as an economic prebiotic.

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Fermented soymilk and soy and cow milk mixture, supplemented with orange peel fiber or Tremella flava fermented powder as prebiotics for high exopolysaccharide‐producing Lactobacillus pentosus SLC 13

Huang

Kao

et al. 2019

J Sci Food Agric

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BACKGROUND: A high exopolysaccharide-producing Lactobacillus pentosus SLC 13 strain was isolated from mustard pickles and showed the characteristics of a probiotic. Orange peel fiber powder (OPFP) and Tremella flava fermented powder (TFP) were shown to be potential prebiotics for L. pentosus SLC 13. The present study aimed to further develop new symbiotic fermented lactic acid beverages using SLC 13 with different proportions of cow milk and soymilk as food substrates, as well as with OPFP or TFP as prebiotics.RESULTS: Acidification rate (soymilk groups, 3.02-4.37 mU min −1 ; soymilk/milk mixture groups, 1.33-2.84 mU min −1 ) and fermentation time (soymilk groups, 7.09-9.25 h; soymilk/milk mixture groups, 12.51-27.34 h) indicated that soymilk represents a suitable substrate for SLC 13-mediated fermentation. Moreover, OPFP and TFP induced a higher exopolysaccharide production of SLC 13 and a higher water holding capacity of fermented beverages. Sensory evaluations suggested that soymilk groups fermented with 10 g kg −1 OPFP (SF-1.0P) and that with 5 g kg −1 TFP (SF-0.5T) and also soymilk/milk mixture groups fermented with 5 g kg −1 OPFP (HSMF-0.5P) and that with 10 g kg −1 TFP (HSMF-1.0T) represent potential fermented drinks. Additionally, SF-1.0P and SF-0.5T products could be preserved for at least 21 days at 4 ∘ C, with high viable cell counts (> 8.8 log 10 CFU mL −1 ) and water holding capacity. CONCLUSION: In the present study, we developed SF-1.0P and SF-0.5T products as a new symbiotic fermented lactic acid beverages. However, in the future, consumer acceptability could be improved by properly regulating the ratio of sugar to acid or seasoning.

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Oxygenated heterocyclic compounds to differentiate Citrus spp. essential oils through metabolomic strategies

Cited by 28 publications

References 44 publications

HPTLC methods for qualitative and quantitative analysis of selected furocoumarins in essential oils

HPTLC methods for qualitative and quantitative analysis of selected furocoumarins in essential oils

Orange Peel Fiber and Tremella flava Fermented Powder Effectively Induce Exopolysaccharide Production by Lactobacillus plantarum SLC

Fermented soymilk and soy and cow milk mixture, supplemented with orange peel fiber or Tremella flava fermented powder as prebiotics for high exopolysaccharide‐producing Lactobacillus pentosus SLC 13

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