1998
DOI: 10.1007/bf02386425
|View full text |Cite
|
Sign up to set email alerts
|

210Pb and210Po analysis in sediments and soils by microwave acid digestion

Abstract: A microwave acid digestion method prior to the determination of 21~ and 21~ in sediments and soils is described. It involves an acid (HNO3, HC1, HF and H3BO 3 mixture) digestion with microwave heating in closed vessels at high pressures. Analyses carried out for various reference materials showed that the results were statistically equal to certified values and reproducibility was also assured. The advantage of the microwave technique compared to the traditional leaching procedures is that the solid materials … Show more

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...
1
1
1
1

Citation Types

1
96
0
3

Year Published

2000
2000
2015
2015

Publication Types

Select...
5
3

Relationship

1
7

Authors

Journals

citations
Cited by 203 publications
(100 citation statements)
references
References 12 publications
1
96
0
3
Order By: Relevance
“…Sediment samples from both the fishing grounds and the control sites at ∼500-m water depth were subsampled (every centimeter down to 10 cm in depth) and freeze-dried, to obtain the vertical profiles of the dry bulk density (ratio of dry weight to volume of the wet sediment slice), as a proxy for sediment compaction. To estimate net accumulation of recently deposited sediments, the activities of the radionuclide 210 Pb (half-life, 22.3 y) were determined by counting the α-emission of its radioactive product 210 Po (56). To obtain the total organic C sedimentary contents (as percentages of total dry weight), aliquots of dried sediment from the top 10 cm of selected sediment were first decalcified by fuming with concentrated HCl for 48 h at 40°C.…”
Section: Methodsmentioning
confidence: 99%
“…Sediment samples from both the fishing grounds and the control sites at ∼500-m water depth were subsampled (every centimeter down to 10 cm in depth) and freeze-dried, to obtain the vertical profiles of the dry bulk density (ratio of dry weight to volume of the wet sediment slice), as a proxy for sediment compaction. To estimate net accumulation of recently deposited sediments, the activities of the radionuclide 210 Pb (half-life, 22.3 y) were determined by counting the α-emission of its radioactive product 210 Po (56). To obtain the total organic C sedimentary contents (as percentages of total dry weight), aliquots of dried sediment from the top 10 cm of selected sediment were first decalcified by fuming with concentrated HCl for 48 h at 40°C.…”
Section: Methodsmentioning
confidence: 99%
“…210 Pb was determined in the first five centimetres of both cores to obtain the most recent maximum sedimentation rates. Determination of 210 Pb activities was accomplished through measurement of its daughter nuclide, 210 Po, following the methodology described by Sánchez-Cabeza et al (1998). Briefly, after addition of a given amount of 209 Po as the internal tracer, sediment aliquots of 200-300 mg of each sample were totally dissolved in an acid medium using an analytical microwave oven.…”
Section: Twomentioning
confidence: 99%
“…Bond et al, 1997;Bianchi and McCave, 1999), Mediterranean (e.g. Casford et al, 2001;Rohling et al, 2009), Tropical Atlantic (e.g. deMenocal et al, 2000Rimbu et al, 2004), and Antarctic deep sea cores (e.g.…”
Section: Introductionmentioning
confidence: 99%
“…Analyses of the sediment samples were performed by total digestion of 200-300 mg using the methodology described by Sanchez-Cabeza et al (1998). 210 Po was added to each sample before digestion, as an internal tracer, and Polonium isotopes were counted with an alpha spectrometer equipped with low-background silicon surface barrier (SSB) detectors (EG&G Ortec).…”
Section: Accepted M Manuscriptmentioning
confidence: 99%
“…The sediment accumulation rate from this core was estimated from 210 Pb concentration profiles. 210 Pb activities were determined through the measurement of its daughter nuclide 210 Po, which is assumed to be in radioactive equilibrium with 210 Pb in the sediment samples, using a method modified after Nittrouer et al (1979).Analyses of the sediment samples were performed by total digestion of 200-300 mg using the methodology described by Sanchez-Cabeza et al (1998). 210 Po was added to each sample before digestion, as an internal tracer, and Polonium isotopes were counted with an alpha spectrometer equipped with low-background silicon surface barrier (SSB) detectors (EG&G Ortec).…”
mentioning
confidence: 99%