2-Amino-4-(4-methoxyphenyl)-1,3-thiazole

Hökelek, Tuncer; Seferoğlu, Zeynel; Ertan, Nermin

doi:10.1107/s1600536806010610

Cited by 5 publications

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“…For the preparation of the title compound, see: Miyaura et al (1979); Finholt et al (1947). For related structures, see: ; Ghabbour, Kadi et al (2012); Hö kelek et al (2006); Yathirajan et al (2006). For bond-length data, see: Allen et al (1987).…”

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confidence: 99%

[2-(Biphenyl-4-yl)-1,3-thiazol-4-yl]methanol

et al. 2012

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Key indicators: single-crystal X-ray study; T = 173 K; mean (C-C) = 0.002 Å; R factor = 0.041; wR factor = 0.114; data-to-parameter ratio = 14.4.In the title compound, C 16 H 13 NOS, the central benzene ring makes dihedral angles of 3.25 (7) and 41.32 (8) , respectively, with the thiazole and phenyl rings. In the crystal, O-HÁ Á ÁN hydrogen bonds link the molecules into a chain along the c axis. A weak C-HÁ Á ÁO interaction further connects the chains into a layer parallel to the ac plane. Related literature

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Section: Related Literaturementioning

confidence: 99%

[2-(Biphenyl-4-yl)-1,3-thiazol-4-yl]methanol

et al. 2012

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“…Comparing (I) with 2-amino-4-(4-methoxyphenyl)-1,3thiazole, (III) (Hö kelek et al, 2006), reveals that all bond lengths and angles of the thiazole ring in (I) are nearly the same. The C2-S1-C5 [88.26 (7) ] bond angle in (I) is smaller than the corresponding one in 2-amino-4-phenylthiazole hydrobromide monohydrate, (IV) (90.17 ; Form et al, 1974), while it is nearly the same as that in (III) [88.4 (3) ].…”

Section: Commentmentioning

confidence: 99%

2-Amino-5-(p-nitrophenylsulfonyl)-1,3-thiazole

et al. 2006

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Crystal structure of 6-(4-chlorophenyl)-6a-nitro-6,6a,6b,7,9,11a-hexahydrospiro[chromeno[3′,4′:3,4]pyrrolo[1,2-c]thiazole-11,11′-indeno[1,2-b]quinoxaline] chloroform monosolvate

et al. 2014

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In the title compound, C33H23ClN4O3S·CHCl3, the thiazole ring adopts an envelope conformation with the N atom as the flap, and the pyrrolidine ring adopts a half-chair conformation. The thiazole ring mean plane makes a dihedral angle of 59.31 (1)° with the pyrrolidine ring mean plane, 71.67 (1)° with the chromene ring and 82.59 (1)° with the chlorobenzene ring. An intramolecular C—H⋯N hydrogen bond occurs. In the crystal, a second C—H⋯N hydrogen bond links the main and solvent molecules. The solvent chloroform molecule is disordered about two positions with an occupancy ratio of 0.508 (14):0.492 (14).

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2-Amino-4-(4-methoxyphenyl)-1,3-thiazole

Abstract: Key indicatorsSingle-crystal X-ray study T = 296 K Mean (C-C) = 0.009 Å R factor = 0.068 wR factor = 0.187 Data-to-parameter ratio = 8.1For details of how these key indicators were automatically derived from the article, see

Cited by 5 publications

References 18 publications

[2-(Biphenyl-4-yl)-1,3-thiazol-4-yl]methanol

[2-(Biphenyl-4-yl)-1,3-thiazol-4-yl]methanol

2-Amino-5-(p-nitrophenylsulfonyl)-1,3-thiazole

Crystal structure of 6-(4-chlorophenyl)-6a-nitro-6,6a,6b,7,9,11a-hexahydrospiro[chromeno[3′,4′:3,4]pyrrolo[1,2-c]thiazole-11,11′-indeno[1,2-b]quinoxaline] chloroform monosolvate

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