2,3-Bis(4-(3-(trifluoromethyl)-3H-diazirin-3-yl)phenyl)oxirane

Wang, Lei; Yoshida, Takuma; Okamoto, Masashi; Sakihama, Yasuko; Hashidoko, Yasuyuki; Hashimoto, Makoto

doi:10.3390/m816

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2015

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“…Their wide ranging importance across chemical sciences has cultivated a great interest in their syntheses [24] through routes using peracids [25], chlorate ions [26] halohydrins [27] or other catalytic methods [28]. Their structures [29,30] vary from simple [31] to asymmetric [32] or as complex systems [33].…”

Section: Introductionmentioning

confidence: 99%

Synthesis of a new bis(perfluoroalkyl oxirane) dioxyethylene ether

Medini

Mekni

Baklouti

2015

Journal of Taibah University for Science

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Classic direct synthetic methods failed to transform bis(perfluororalkylallyl) dioxyethylene ether into the corresponding bis(perfluoroalkyl oxirane). This transformation was instead realized using a mixture of mercuric acetate/bromine to produce the corresponding bromoacetate, which was subsequently transformed to a bromohydrin and further to bis(perfluoroalkyl oxirane) through the use of triethylbenzyl ammonium chloride as a phase transfer catalyst in alkaline media.

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