1H and13C NMR study of some polychlorobuta-1,3-diene derivatives

10 Cl (Br)Cl Cl Br S Br O 12 R 2 5 R 1 S R 1 S H Cl Cl Cl 4 Cl H Cl Cl Cl R 1 S Abstract Thiosubstituted butadiene and butenyne compounds were synthesized from the reactions of 1,1,3,3,4,4-hexachloro-1-butene or 1,1,2,4,4-pentachlorobuta-1,3-diene with different thiols in EtOH/H 2 O solution of NaOH. Tris(thio)substituted butadiene compound was treated with potassium tert-butoxide to obtain tris(thio)substituted butatrienyl halide compound. The novel sulfoxide compounds were synthesized from the reactions of polyhalobutadiene compounds with aliphatic thiols in CHCl 3 with m-CPBA at 0 • C. The structures of the novel compounds were characterized by micro analysis, FT-IR, 1 H-NMR, 13 C-NMR, and MS.

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Synthesis of Novel Thioethers and Sulfoxide Compounds

Ibis

Ayla

Beyazit

et al. 2013

Phosphorus, Sulfur, and Silicon and the Related Elements

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1H and13C NMR study of some polychlorobuta-1,3-diene derivatives

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Synthesis of Novel Thioethers and Sulfoxide Compounds

Synthesis of Novel Thioethers and Sulfoxide Compounds

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