13-Acetoxy-heptadecadien-(8, 10)-ol-(1), Octadien-(3, 5)-ol-(1)-Isomere und verwandte Verbindungen

Riemschneider, R.; Kasang, G.; Böhme, Chr.

doi:10.1007/bf01185898

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1971

1993

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Cited by 5 publications

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“…Glc (2.5% SE-30 on Chromosorb G AW-DMCS) showed isomer ratio trans:cis 96:4. Spinning-band distn gave 16.01 g (containing 0.83% cis) of 4 (R = Si(CH3)3), bp 70-74°(1.8 mm). Anal.…”

Section: Methodsmentioning

confidence: 99%

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Synthesis of fatty acids with smooth muscle stimulant activity. 3. Acetylenic analogs of 12-hydroxyheptadeca-trans-8,trans-10-dienoic acid

Crundwell¹,

Cripps²

1972

J. Med. Chem.

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Crundwell and Cripps (C20H26N2) C, , N. The maleate salt, mp 127-130°, was recrystd from ;-PrOH-Et20. Anal. (C20H26N2-C4H4O4) C, , N. Acknowledgment. The authors are indebted to the members of the Biological Division of the Schering Corp.for the biological results herein reported and for permission to use some of their data. We are especially indebted to Dr.Irving I. Tabachnick, the late Dr. Franklin Roth, and Mr. Salvatore Tozzi and their staffs for the antianaphylactic and antihistamine data. References(1) F.

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“…Glc (2.5% SE-30 on Chromosorb G AW-DMCS) showed isomer ratio trans:cis 96:4. Spinning-band distn gave 16.01 g (containing 0.83% cis) of 4 (R = Si(CH3)3), bp 70-74°(1.8 mm). Anal.…”

Section: Methodsmentioning

confidence: 99%

“…(CI0H1SC1) C, H. Cl. 16-Chlorohexadec-/rzzns-9-en-7-yn-6-ol (11, X = Q). The bromomagnesium derivative of 10 (2.99 g, 0.0175 mole) reacted with 1-hexanal (2.46 g, 0.025 mole) under conditions similar to those described29 to give 4.27 g (90%) of 11 (X = Cl), bp 137-144°(0.005 mm).…”

Section: Methodsmentioning

confidence: 99%