Matrix Solid-Phase Dispersion<i>versus</i>Ultrasound Assisted Extraction with Solid-Phase Extraction in the HPLC Analysis of Furanocoumarins from Fruits of<i>Archangelica officinalis</i>Hoffm.

Oniszczuk, Anna; Skalicka-Woźniak, Krystyna; Oniszczuk, Tomasz; Waksmundzka‐Hajnos, Monika; Głowniak, Kazimierz

doi:10.5935/0103-5053.20140093

Cited by 2 publications

(4 citation statements)

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“…An alternative to conventional methods for isolating furanocoumarin from fruit was proposed by Oniszczuk et al [20]. The yield was prepared by matrix solid-phase dispersion (MSPD) method compared with ultrasonification with solid-phase extraction (USAE-SPE) and then HPLC analyses were performed.…”

Section: Results Of the Study Indicate That The Level Of Furanocumarimentioning

confidence: 99%

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Variability of composition of essential oil and coumarin compounds of Angelica archangelica L.

Forycka

Buchwald

2019

Herba Polonica

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SummaryThe medicinal and culinary properties of Angelica archangelica L. have been known and valued since the Middle Ages. Ingredients of essential oil and coumarins found in this plant are to a large degree responsible for its pharmacological activity. This study is a review of the literature of the most important biologically active compounds present in herbal raw materials: root (rhizome with roots) and angelica fruits. Research shows that the content of individual compounds of the essential oil and coumarin fraction is variable, which may point to a large intraspecific variation. Therefore, these compounds may be good markers for identifying taxa or chemotypes in chemotaxonomic research valuable for the herbal medicine and pharmaceutical industry.

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Section: Results Of the Study Indicate That The Level Of Furanocumarimentioning

confidence: 99%

“…The fruits of angelica were previously used in smaller scale. Nowadays, they are considered to be a rich source of coumarin compounds with potentially wide range of applications in various therapeutic purposes [3,[18][19][20].…”

Section: Introductionmentioning

confidence: 99%

Variability of composition of essential oil and coumarin compounds of Angelica archangelica L.

Forycka

Buchwald

2019

Herba Polonica

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“…Method limit of detection (LOD) (ng ml -1 ) and limit of quantification (LOQ) (ng ml -1 ) in spiked river water (n = 3). acetate-ionic liquid dispersive liquid-liquid micro extraction high performance liquid chromatography coupled to variable wavelength UV detector (EA-IL-DLLME-HPLC-UV) (Dongli et al, 2014) Aluminium hydroxide co-precipitation coupled to high performance liquid chromatography with UV detection (AH-C-HPLC-UV) (Yang et al, 2013), dispersive solid phase microextraction coupled to high performance liquid chromatography-diode-array detection (DSPM-HPLC-DAD) (Tsai et al, 2009), online solid phase extraction coupled to high performance liquid chromatography with photodiode array detection (on line HPLC-PAD) (Oniszczuk et al, 2014) see Table 4.…”

Section: Limit Of Detection (Lod) and Limit Of Quantification (Loq)mentioning

confidence: 99%

“…Dispersive solid phase extraction (DSPE) and matrix solid phase dispersion (MSPD) are techniques that have been developed recently and have been found to be very versatile (Tsai et al, 2009). Recoveries greater than 97% were reported when tetracyclines in food samples were determined by these techniques (Oniszczuk et al, 2014). These methods have been found to be quick, easy, cheap, rugged and use less solvents.…”

Section: Introductionmentioning

confidence: 99%

Extraction of tetracycline antimicrobials from river water and sediment: a comparative study of three solid phase extraction methods

Dzomba¹,

Kugara²,

M³

2015

Afr. J. Pharm. Pharmacol.

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Tetracyclines are ubiquitous pollutants in the aquatic environment so it is necessary to determine their levels in river water and sediment. Many extraction techniques have been suggested in previous studies. However there is lack of comparisons among them. This work compared three extraction methods Ultrasonic Assisted Tandem Solid Phase Extraction (UA-TSPE), Ultrasonic Assisted Dispersive Solid Phase Extraction (UA-DSPE) and Ultrasonic Assisted Matrix Solid Phase Dispersion (UA-MSPD) in conjunction with a complexing agent to complex metal cations, for the extraction of tetracycline antibacterials from fortified ultra-pure water, river water and sediment samples under acid conditions. Samples were analyzed on a RP-HPLC coupled to UV detection. The linear dynamic range for calibration curves of all techniques were 0.01 to 1 µgml-1 (water) and 0.01 to 1 µgg-1 (sediment) with R 2 values ranging from 0.995 to 0.999. The overall recovery was in the range 92.13 to 99.62%. UA-DSPE yielded the best recoveries (at p > 0.05), range 97.23 to 99.62%. UA-TSPE was second at 94.99 to 97.75%, while UA-MSPD was third at 92.13 to 97.84% recovery. Limit of detection (LOD) (at signal to noise ratio = 3) and Limit of quantification (LOQ) (at signal to noise ratio = 10) for spiked river water and sediment were in the range 11.53 to 22.75 ngml-1 and 30.12 to 56.22 ngml-1 , respectively.

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Matrix Solid-Phase DispersionversusUltrasound Assisted Extraction with Solid-Phase Extraction in the HPLC Analysis of Furanocoumarins from Fruits ofArchangelica officinalisHoffm.

Cited by 2 publications

References 0 publications

Variability of composition of essential oil and coumarin compounds of Angelica archangelica L.

Variability of composition of essential oil and coumarin compounds of Angelica archangelica L.

Extraction of tetracycline antimicrobials from river water and sediment: a comparative study of three solid phase extraction methods

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