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Arslan, Hakan

doi:10.5155/eurjchem.3.3.i-i.679

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2013

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“…The two naphthyl planes make dihedral angles of 76.16(8)/59.63(7)° (molecule A/B). In general, there are no unexpected geometric parameters if this structure is compared to similar thiourea compounds, for example, bis[2,2‐diphenyl‐ N ‐(di‐ n ‐propylcarbamothioyl)acetamido]copper(II)13 and bis[4‐bromo‐ N ‐(di‐ n ‐butylcarbamothioyl)benzamido]copper(II) 13. The S‐parameter (Goof, goodness of fit) normally lies in the 0.7–1.0 range.…”

Section: Resultsmentioning

confidence: 99%

Phase‐Controlled Deposition of Copper Sulfide Thin Films by Using Single‐Molecular Precursors

et al. 2013

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Herein, we describe the synthesis and characterization of new ligands, N, and N,N-dipropyl-NЈ-(1-naphthoyl)thiourea (1b), and their complexes with copper, bis[N,N-diethyl-NЈ-(1-naphthoyl)thioureato]Cu II (2a) and bis[N,N-dipropyl-NЈ-(1-naphthoyl)thioureato]Cu II (2b). All four compounds (i.e., 1a, 1b, 2a, and 2b) were characterized by elemental analysis, 1 H NMR and 13 C NMR spectroscopy, and FTIR spectroscopy. The structures of compounds 1a, 1b, and 2b were determined by single-crystal X-ray diffraction analysis. Thermogravimetric analysis of 2a and 2b showed that both compounds decompose between [a]

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Section: Resultsmentioning

confidence: 99%