2018
DOI: 10.1590/0104-6632.20180353s20160724
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Optimization of Preparation Conditions for Activated Carbons From Polyethylene Terephthalate Using Response Surface Methodology

Abstract: This work proposes the optimal conditions for the preparation of activated carbons from polyethylene terephthalate (PET) with good surface area and yield. The PET-based activated carbon was prepared using a chemical activation technique employing sulfuric acid (H 2 SO 4). Different preparation conditions involving impregnation ratio, activation temperature and activation time were investigated to evaluate their effects on both surface area and yield. The central composite design (CCD) approach was adopted to d… Show more

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Cited by 18 publications
(3 citation statements)
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“…CCD was used in this study to assess the impact of reaction temperature ( T ) and residence time ( t ) on the fuel characteristics. RSM/CCD is suitable for the optimization of process parameters and the analysis of the interaction between these parameters. The structure and design matrix of the HTC experiments are shown in Table with 11 experimental runs. There are four factorial points, four axial points, and three center points, which were repeated five times to obtain an accurate estimate of the experimental error and data reproducibility.…”
Section: Methodsmentioning
confidence: 99%
“…CCD was used in this study to assess the impact of reaction temperature ( T ) and residence time ( t ) on the fuel characteristics. RSM/CCD is suitable for the optimization of process parameters and the analysis of the interaction between these parameters. The structure and design matrix of the HTC experiments are shown in Table with 11 experimental runs. There are four factorial points, four axial points, and three center points, which were repeated five times to obtain an accurate estimate of the experimental error and data reproducibility.…”
Section: Methodsmentioning
confidence: 99%
“…This may be attributed to the uniform micropores developed by the carbon-water reaction. However, with the increase of activation temperature, the micropores were enlarged to mesopores and macropores, thereby reducing the adsorption capacity of iodine to some extent (Sureshkumar & Susmita 2018). The iodine adsorption capacity of FRAC initially increased and thereafter declined with the prolongation of activation time, which could be seen from Figure 1(a) and 1(c).…”
Section: D Response Surface Plot Analysismentioning
confidence: 89%
“…Após pirolise da matéria-prima de CSA (Figura 2) sob aquecimento até a temperatura de 450°C, o rendimento de carvão adsorvente foi de 28,82%. De acordo com Ayyalusamy & Mishra (2018), a temperatura de pirólise pode alterar drasticamente o rendimento de carvão, sendo um parâmetro para otimização do processo, porém, a temperatura de pirólise escolhida neste trabalho se mostrou favorável no rendimento de carvão adsorvente.…”
Section: Análise Preliminar Da Matéria-prima De Csaunclassified