1998
DOI: 10.1107/s0108270197017514
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1,4-Bis[3-(N-ethyliminomethyl)-2-hydroxy-5-methylbenzyl]piperazine

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Cited by 6 publications
(8 citation statements)
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“…The bond lengths observed in the two phenyl rings agree with each other and are comparable with average values reported in the literature (Domenicano et al, 1975;Allen et al, 1987). The bond lengths and angles observed in the piperazine ring are comparable with those of related reported structures (Gunasekaran et al, 1996;Thirumurugan et al, 1998). The bond lengths C23ÐN24 and C30Ð N31, which are 1.260 (2) and 1.252 (3) A Ê , respectively, indicate a double-bond character (Thirumurugan et al, 1998).…”
supporting
confidence: 90%
See 1 more Smart Citation
“…The bond lengths observed in the two phenyl rings agree with each other and are comparable with average values reported in the literature (Domenicano et al, 1975;Allen et al, 1987). The bond lengths and angles observed in the piperazine ring are comparable with those of related reported structures (Gunasekaran et al, 1996;Thirumurugan et al, 1998). The bond lengths C23ÐN24 and C30Ð N31, which are 1.260 (2) and 1.252 (3) A Ê , respectively, indicate a double-bond character (Thirumurugan et al, 1998).…”
supporting
confidence: 90%
“…they adopt Àantiperiplanar and +antiperiplanar conformations with respect to one another. The torsion angles C5ÐC6ÐC7ÐN8 and C16ÐC15ÐC14ÐN11 [76.6 (2) and À78.3 (2) , respectively] de®ne the orientation of the substituents on the piperazine ring; both are in equatorial positions and the molecule thus has an extended conformation and is pseudocentrosymmetric (Thirumurugan et al, 1998).…”
mentioning
confidence: 99%
“…2. The piperazine ring exhibits a chair conformation with the usual bond lengths and angles (Yogavel et al, 2003), comparable with those of related reported structures (Gunasekaran et al, 1996;Thirumurugan et al, 1998).…”
Section: S1 Commentsupporting
confidence: 88%
“…For the synthesis of related compounds, see: Zheng et al (2005); Sarangarajan et al (2005). For related structures, see: Yogavel et al (2003); Gunasekaran et al (1996); Thirumurugan et al (1998).…”
Section: Related Literaturementioning
confidence: 99%
“…All the bond lengths and bond angles are in the normal range. The bond length N(3)-C(5) (1.288(4) Å ) indicates a doublebond character [24]. The imidazolyl rings are located antiparallely above and below the benzene planes, respectively.…”
Section: Resultsmentioning
confidence: 99%