1-(3-Isoselenocyanatopropyl)adamantane

Pitushkin, D. A.; Burmistrov, V. V.; Бутов, Г. М.

doi:10.3390/m1646

Molbank

2023

DOI: 10.3390/m1646

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1-(3-Isoselenocyanatopropyl)adamantane

D. A. Pitushkin

V. V. Burmistrov

Г. М. Бутов

Abstract: The title compound, 1-(3-isoselenocyanatopropyl)adamantane, was synthesized for the first time from 3-(adamantan-1-yl)propan-1-amine by the two-stage reaction with 1-(3-isocyanopropyl)adamantane as intermediate. The product was characterized by NMR, GC-MS, and elemental analysis.

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2024

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A New Method for the Synthesis of 1-(1-Isocyanoethyl)adamantane

Pitushkin,

Butov

2024

Molbank

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A novel single-step method has been developed for the synthesis of 1-(1-isocyanoethyl)adamantane from 1-(1-adamantylethyl)amine, chloroform, and t-BuOK, in a dichloromethane/tert-butanol (1:1) medium, yielding 92%, which is 27% higher compared to the known method, without the use of highly toxic compounds. The product was characterized using 1H and 13C NMR spectroscopy, GC-MS, and elemental analysis.

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A New Method for the Synthesis of 1-(1-Isocyanoethyl)adamantane

Pitushkin,

Butov

2024

Molbank

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1-(3-Isoselenocyanatopropyl)adamantane

Abstract: The title compound, 1-(3-isoselenocyanatopropyl)adamantane, was synthesized for the first time from 3-(adamantan-1-yl)propan-1-amine by the two-stage reaction with 1-(3-isocyanopropyl)adamantane as intermediate. The product was characterized by NMR, GC-MS, and elemental analysis.

Cited by 1 publication

References 19 publications

A New Method for the Synthesis of 1-(1-Isocyanoethyl)adamantane

A New Method for the Synthesis of 1-(1-Isocyanoethyl)adamantane

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