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A numerical algorithm is developed to simulate the injection-compression molding (ICM) process. A Hele-Shaw fluid-flow model combined with a modified control-volume/finite-element method is implemented to predict the melt-front advancement and the distributions of pressure, temperature, and flow velocity dynamically during the injection melt filling, compression melt filling, and postfilling stages of the entire process. Part volumetric shrinkage was then investigated by tracing the thermal-mechanical history of the polymer melt via a path display in the pressure-volumetemperature (PVT) diagram during the entire process. Influence of the process parameters including compression speed, switch time from injection to compression, compression stroke, and part thickness on part shrinkage were understood through simulations of a disk part. The simulated results were also compared with those required by conventional injection molding (CIM). It was found that ICM not only shows a significant effect on reducing part shrinkage but also provides much more uniform shrinkage within the whole part as compared with CIM. Although using a higher switch time, lower compression speed, and higher compression stroke may result in a lower molding pressure, however, they do not show an apparent effect on part shrinkage once the compression pressure is the same in the compression-holding stage. However, using a lower switch time, higher compression speed, and lower compression stroke under the same compression pressure in the postfilling stage will result in an improvement in shrinkage reduction due to the melt-temperature effect introduced in the end of the filling stage.

Objectives This study presents a variant of the Brazilian disk test (BDT) for assessing the bond strength between composite resins and dentin. Methods Dentin-composite disks (φ 5 mm × 2 mm) were prepared using either Z100 or Z250 (3M ESPE) in combination with one of three adhesives, Adper Easy Bond (EB), Adper Scotchbond Multi-Purpose (MP) and Adper Single Bond (SB), and tested under diametral compression. Acoustic emission (AE) and digital image correlation (DIC) were used to monitor debonding of the composite from the dentin ring. A finite element (FE) model was created to calculate the bond strengths using the failure loads. Fracture modes were examined by scanning electron microscopy (SEM). Results Most specimens fractured along the dentin-resin composite interface. DIC and AE confirmed interfacial debonding immediately before fracture of the dentin ring. Results showed that the mean bond strength with EB (14.9±1.9 MPa) was significantly higher than with MP (13.2±2.4 MPa) or SB (12.9±3.0 MPa) (p<0.05); no significant difference was found between MP and SB (p>0.05). Z100 (14.5±2.3 MPa) showed higher bond strength than Z250 (12.7±2.5 MPa) (p<0.05). Majority of specimens (91.3%) showed an adhesive failure mode. EB failed mostly at the dentin-adhesive interface, whereas MP at the composite-adhesive interface; specimens with SB failed at the composite-adhesive interface and cohesively in the adhesive. Conclusions The BDT variant showed to be a suitable alternative for measuring the bond strength between dentin and composite, with zero premature failure, reduced variability in the measurements, and consistent failure at the dentin-composite interface.

Objective To verify and calibrate a chemical model for simulating the degradation of the dentin-composite interface induced by multi-species oral biofilms in vitro. Methods Dentin-composite disks (5-mm dia. × 2-mm thick) were made from bovine incisor roots and filled with either Z100™ (Z100) or Filtek™ LS (LS) composite. The disks, which were covered with nail varnish, but with one of the dentin-composite margins exposed, were immersed in lactic acid solution at pH 4.5 for up to 48 hr. Diametral compression was performed to measure the reduction in bond strength of the dentin-composite disks following acid challenge. Scanning electron microscopy (SEM) was used to examine decalcification of dentin and fracture modes of the disks. To better understand the degradation process, micro-computed tomography, in combination with a radiopaque dye (AgNO3), was used to assess interfacial leakage in 3D longitudinally, while SEM was used to determine the path of leakage. One-way analysis of variance (ANOVA) was used to analyze the results, with the level of statistical significance set at p < 0.05. The results were compared with those obtained previously using multi-species biofilms for verification and calibration purposes. Results After 48 hr of acid challenge, the debonding load of both the LS- and Z100-filled disks reduced significantly (p < 0.05). In the Z100-filled disks, debonding mostly occurred at the adhesive-dentin interface, while in the LS-filled disks, this happened at the adhesive-composite interface, instead. The degree of dentin demineralization, the reduction in debonding load and the modes of failure observed were very similar to those induced by multi-species oral biofilms found in the previous work. Leakage of AgNO3 occurred mainly along the hybrid layer. The specimens filled with Z100 had a thicker hybrid layer (∼6.5 μm), which exhibited more interfacial leakage than those filled with LS. Significance The chemical model with lactic acid used in this study can induce degradation to the dentin-composite interface similar to those produced by multi-species biofilms. With appropriate calibration, this could provide an effective in vitro method for ageing composite restorations in assessing their potential clinical performance.