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Graphene has been regarded as a potential application material in the field of new energy conversion and storage because of its unique two-dimensional structure and excellent physical and chemical properties. However, traditional graphene preparation methods are complicated in-process and difficult to form patterned structures. In recent years, laser-induced graphene (LIG) technology has received a large amount of attention from scholars and has a wide range of applications in supercapacitors, batteries, sensors, air filters, water treatment, etc. In this paper, we summarized a variety of preparation methods for graphene. The effects of laser processing parameters, laser type, precursor materials, and process atmosphere on the properties of the prepared LIG were reviewed. Then, two strategies for large-scale production of LIG were briefly described. We also discussed the wide applications of LIG in the fields of signal sensing, environmental protection, and energy storage. Finally, we briefly outlined the future trends of this research direction.

In this study, a special core–shell structured wool-TiO2 (WT) hybrid composite powder also having TiO2 nanoparticles incorporated inside cortical cells was reported. The wool pallets were pulverized from wool fibers using vibration-assisted ball milling technique and the WT powders having mesopores and macropores were produced in hydrothermal process. Experimental results indicated that the infiltrated TiO2 nanoparticles were amorphous structure, while the coated TiO2 nanoparticles were anatase phase structure. The crystallized TiO2 nanoparticles were grafted with wool pallets by the N−Ti4+/S−Ti4+/O−Ti4+ bonds. The BET surface area was measured as 153.5 m2/g and the particle sizes were in the 600–3600 nm and 4000–6500 nm ranges. The main reactive radical species of the WT powders were holes, and •O2−, 1O2, and •OH were also involved in the photodegradation of MB dye under visible light irradiation. The experimental parameters for photodegradation of MB dye solution were optimized as follows: 0.25 g/L of WT powders was added in 40 mL of 3 mg/L MB dye solution containing 50 mL/L H2O2, which resulted in the increases of COD value of degraded MB dye solution up to 916.9 mg/L at 120 min. The WT powders could be used for repeatedly photodegradation of both anionic and cationic dyes.

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