Ill] L. M. Litrinenko, V. A. Dadli, V. A. Sarelora, T. I. Krichertsora, J. Gun.Chrm., USSR (Engl. Transl.) 1964,34, 3780. [12] Satisfactory elemental analyses were obtained for all new compounds. 2, yield 61 YO, m.p. 128°C (decomp.), IR (KBr, vjcm-') 1455, 1065, 1040, 880,441; '3CC-NMR(DMS0)219.2,89.5;MSm/z386(Mm).3:yield89%, m.p. 97°C (decomp.); IR (KBr, vjcm-') 1652, 1612, 1485, 881,445; "C-NMR (DMSO) 198.3, 80.0; MS m/z 370 (M"). 4: yield 68%, m.p. 175°C (decomp.); IR (KBr, sjcm-') 833,765,701,668,442; I3C-NMR (DMSO) 116.7, 79.9; MS mjz 708 (Me); HRMS calc. for C,I,S,: 707.5057, found 707.5052. [13] Crystal data for 5: C,I,S,, Mw = 834.84, monoclinic, space group C2/c, u = 9.033(2), b = 13.974(6), c = 14.002(5) A, p = 104.24(2)", V = 1713.2 A3, 2 = 4, D, = 3.237 gem-), p = 94.3 cm-', F (000) = 1460, 2Q,,, = 46 ', o-scan, crystal dimensions 0.17 x 0.30 x 0.47 mm, graphite monochromated Mo-Kz radiation, L = 0.71069 A. The data were collected on an Enraf-Nonius CAD4 diffractometer. The structure was solved by direct methods using SIR88 in MOLEN and refined by least-squares full matrix (anisotropic for non-hydrogen atoms) to R = 0.018, R, = 0.031 for 1103 observed reflections with I > 3u(/) out of 1246 unique data, 69 variables. Supplementary material on the X-ray structure determination may be obtained from the Fachinformationszentrum Karlsruhe, Gesellschaft fur wissenschaftlich-technische Information mbH, D-76344 Eggenstein-Leopoldshafen 2, on quoting the names of the authors and the journal citation. [14] T.