In this study, magnetic iron oxide/graphene oxide (Fe 3 O 4 /GO) nanocomposites were developed for removal of cadmium ions (Cd 2+ ) from water, which could be effectively separated from the solution owing to its superparamagnetic property. The Fe 3 O 4 /GO nanocomposites were fabricated by coprecipitation method with different precursor ratios of 8:1, 4:1, 2:1, and 1:1. It was found that the suitable ratio of Fe 3 O 4 /GO for Cd 2+ ions adsorption was 4:1 (FG2). The effects of contact time, pH, and metal initial concentration on the adsorption properties of FG2 for Cd 2+ in water were investigated. The adsorption data of FG2 followed pseudo-second-order kinetic and Langmuir isotherm models with the maximum adsorption capacity of 52.083 mg g −1 at pH 8. The structure and morphology of FG2 were characterized by X-ray diffraction, Fourier transform infrared spectroscopy, transmission electron microscopy (TEM), Brunauer-Emmett-Teller (BET) specific surface area, and vibrating sample magnetometry (VSM). TEM images of FG2 presented the Fe 3 O 4 nanoparticles in the size range of 10-15 nm decorated on GO nanosheets. The BET specific surface area of FG2 was observed to be 180.84 m 2 g −1 . VSM result of FG2 was 41.13 emu g −1 . Accordingly, FG2 could be considered as a highly efficient adsorbent for removing Cd 2+ from water.
In this study, to investigate the extraction of triterpenoids from the Vietnamese red G. lucidum by ultrasound‐assisted extraction (UAE) method using ethanol as a solvent, the determination of the four single factors influence on the triterpenoid content including liquid‐to‐solid ratio, extraction power, extraction temperature, and extraction time was carried out for the performance of experiments on simultaneous effects by Central Composite design. The results showed that based on ultraviolet‐visible spectroscopy analysis, the highest yield of triterpenoids could be achieved with value of 18.3751 mg/g under optimal extraction conditions including extraction time of 60 min, ultrasonic power of 360 W, liquid‐to‐solid ratio of 38 : 1 mL/g, and ultrasonic temperature of 48 °C. To determine the characteristics of the obtained extract, the Gas chromatography‐mass spectrometry, the Fourier‐transform infrared spectroscopy, scanning electron microscope, and the thermogravimetric analyzer were employed in this study. Besides, for antioxidant capacity evaluation, the DPPH free radical scavenging assay, H2O2 scavenging assay, and the ABTS radical cation decolorization assay were carried out whereas the anticancer evaluation results denoted the potential for anticancer agents of G. lucidum extract. Therefore, it could be concluded that UAE is a promising method for triterpenoid extraction with antioxidant properties.
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