The mixed-valent cyclic trinuclear cobalt(II)/cobalt(III)/cobalt(III) complex tris(dibenzoylmethanato-1κ 2 O,OЈ;2κ 2 O,OЈ;3 κ 2 O,OЈ)(µ 3 -hydroxo-1:2κ 2 O;1:3κ 2 O;2:3κ 2 O)tetrakis(µ-pyrazolato-1:2κ 4 N 1 N 2 ;1:3κ 2 N 1 N 2 ;2:3κ 2 N 1 N 2 )-1,2-dicobalt-(III)-3-cobalt(II) with four bridging pyrazolate anions and a µ 3 -hydroxy anion has been synthesized and its molecular structure has been elucidated on the basis of X-ray crystallographic, magnetic, NMR, and EPR studies. The remaining coordination sites of the pentacoordinate cobalt(II) and hexa-
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