A new method for characterising the rate-dependent failure of elasto-plastic adhesively bonded structures has been developed and used to investigate the different modes of loading of representative interfaces. Furthermore, experimental observations enabled a newly developed cohesive zone model that captures all critical aspects of the observed and quantified behaviour of the adhesive under consideration. In particular, the model is capable of reproducing the conducted experiments by incorporating both the dependence of the deformation rate and the adhesive thickness. For that, computed tomography of the adhesive interface was used to resolve three-dimensionally the adhesive volume. The volume fraction of microscopic voids in the adhesive was introduced into the model to rationalise the observed dependence of the mechanical response of the adhesive upon its thickness. Finally, the cohesive zone model was proven with mixed-mode fracture experiments which demonstrate the model's ability to simulate more complex deformation regimes.
Fracture mechanics experiments are used to investigate the rate-dependent failure of adhesively bonded structures under different deformation modes: I, II and I/II. First, the high-rate mechanical response of the adhesive interface is analysed with a newly developed method -which relies entirely upon digital image correlation. The method was purposely designed to avoid any dynamic effects which may be present. This novel method is verified against quasi-static standard methods showing good agreement. Finally, simulations of the experiments are used to validate a cohesive zone model of the adhesive. The ability of the model to predict cohesive failure under a wide range of strain rates and deformation modes is demonstrated.
The increasing use of adhesive joints in dynamic applications require reliable measurements of the rate-dependent stress-displacement behaviour. The direct measurement of the stress-displacement curve is necessary when using cohesive models in discretised solutions of boundary value problems in solid mechanics. This paper aims to investigate the rate-dependent tensile failure of adhesive joints by using a new experimental methodology-it relies upon the combination of the stress wave propagation theory and digital image correlation methods on high speed footage to quantify the tensile stress and the dissipated energy respectively. For this purpose, the Split Hopkinson Bar methodology was employed-the experimental configuration was optimised using numerical modelling. To prove the sensitivity of our framework, two different adhesives are characterised at different loading rates: the adhesive failure strength was found to increase considerably with the strain rate, while the plastic deformation of these adhesives was reduced. The film adhesive showed superior performance over the particle toughened one. In the final part, a rate-dependent cohesive zone model is proposed, one which captures the measured behaviour and which has the potential to be used in industrial applications.
Electrospinning technique is well-known for the generation of different fibers. While it is a "simple" technique, it lies in the fact that the fibers are typically produced in the form of densely packed two-dimensional (2D) mats with limited thickness, shape, and porosity. The highly demanded threedimensional (3D) fiber assemblies have been explored by timeconsuming postprocessing and/or complex setup modifications. Here, we use a classic electrospinning setup to directly produce 3D fiber macrostructures only by modulating the spinning solution. Increasing solution conductivity modifies electrodynamic jet behavior and fiber assembling process; both are observed in situ using a high-speed camera. More viscous solutions render thicker fibers that own enhanced mechanical stiffness as examined by finite element analysis. We reveal the correlation between the universal solution parameters and the dimensionality of fiber assemblies, thereof, enlightening the design of more "3D spinnable" solutions that are compatible with any commercial electrospinning equipment. After a calcination step, ultralightweight ceramic fiber assemblies are generated. These inexpensive materials can clean up exceptionally large fractions of oil spillages and provide high-performance thermal insulation. This work would drive the development and scale-up production of next-generation 3D fiber materials for engineering, biomedical, and environmental applications.
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