At.Spectrosc. volume 36, issue 3, P146-151 2015 DOI: 10.46770/as.2015.03.006 View full text
M.A. Habila, M. Soylak

Abstract: A Fe 3 O 4 nanoparticle and ultrasonic coupled dispersive liquidliquid microextraction (NPsU-DLLME) method was developed for the preconcentration of lead from water, tobacco, and fertilizer samples. Imidazole-2,4-dicarboxylic acid was used as the chelating agent and carbon tetrachloride as the extractor solvent. Addition of certain amounts of Fe 3 O 4 nanoparticles and specific exposure periods to ultrasonic waves were optimized. Maximum recovery (%) was obtained using the following conditions: 17.5 mL sample …

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