1906
DOI: 10.1002/cber.19060390144 View full text |Buy / Rent full text
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Abstract: Einwirkung von Aldehyden auf O r t h o d i a m i n e der Pyrimidinreihe. [Aus dem pharmaceutischen Institut der UniversitLt Berlin.] (Eingegangen a m 11. Januar 1906.) Der Eine von uns hat vor einigen Jahren das Xanthin und riele diesem verwandte Verbindungen durch Eiuwirlrung o r g a n i s c h e r Sii u r e n auf gewisse o-D i a m i n 0-p y r i m i d i n e dargestellt I). Neuerdings haben wir gefunden, dass man zu Xanthinbasen auch gelangen kann durch Einwirkung VOII A l d e h y d c n auf dieselben Diamine de… Show more

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“…After cooling, the precipitated crystal was collected by filtration, dried in the oven and recrystallized from appropriate solvent to give 5a-g. 5a: m. 5-Amino-6-methylamino-1-methyluracil (8). 18 This compound was prepared as a reported method. 1-Methyl-6-Methylamino-5-(4-trifluoromethylbenzamido)-uracil (9e).…”
Section: Methodsmentioning
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“…After cooling, the precipitated crystal was collected by filtration, dried in the oven and recrystallized from appropriate solvent to give 5a-g. 5a: m. 5-Amino-6-methylamino-1-methyluracil (8). 18 This compound was prepared as a reported method. 1-Methyl-6-Methylamino-5-(4-trifluoromethylbenzamido)-uracil (9e).…”
Section: Methodsmentioning
“…3,9-dimethylxanthines has been prepared by various methods. [10][11][12][13] 8-Arylpurines have been synthesized either by dehydrocyclization of 4-amino-5-arylamidopyrimidines with phosphoryl chloride, 14,15 phosphoric acid 16 and by dry heating, 17 or by cyclization of Schiffs base analogues using ferric chloride, 18 nitrobenzene, 19 or bisulfite adduct of aldehydes. 20 We report herein the synthesis of some purine analogues, namely 3,9-dimethyl-, and 8-aryl-3,9-dimethylxanthines.…”
mentioning
“…Cyanuric Acid as a Pseudo-acid. ARTHUR HANTZSCH (Ber., 1906, 39, 139-153. Compare Ponomareff, Abstr., 1886.-Cyanuric acid is a tricarbimide, and as a complete pseudo-acid should be termed pseudocyanuric acid.…”
Section: Smentioning
“…EMILIO NOELTING and E. 0. SOMMERHOFF (Ber., 1906 , 39, 76-79. Compare Hepp, Abstr., 1883, 315 ; van Romburgh, Abstr., 1895, i, 652 ; Sudborough, Trans., 1901, 79, 522 ;Sschs and Steinert, Abstr., 1904, i, 506).-The authors have prepared a number of additive compounds from 1 mol.…”
Section: E Gmentioning
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