Thermal decomposition of N-(salicylidene)-L-leucine in static air atmosphere

Abstract

The thermal degradation of N-(salicylidene)-L-leucine was studied under non-isothermal conditions in air atmosphere. For kinetic analysis, the TG/DTA/DTG data obtained at three different heating rates were processed by Friedman, Kissinger-Akahira-Sunose, Flynn-Wall-Ozawa and Kissinger methods. The analysis indicates a complex reaction process which can be best described by the three dimensional (Ginstling-Brounshtein) model D4.

The kinetic analysis of non-isothermal carisoprodol reaction in nitrogen atmosphere using the invariant kinetic parameters method

“…DTA curves for the thermal decomposition of carisoprodol in nitrogen atmosphere at different heating rates(5,10,15, and 20 °C/min).…”

“…The invariant kinetic parameters (IKP) method was applied to study thermal decomposition of few pharmacologically active compounds, e.g. N,N'-bis (3,5-di-t-butylsalicylidene)-1,3-ethylene-diamine metal complexes [9] and N-(salicylidene)-L-leucine [10].…”

Pyrolysis, Kinetic and Kinetic Model Study of Epoxidized Natural Rubber

“…Adjustment methods can provide some information about the degree of kinetic control. Model-fitting methods such as Friedman Isoconversional [6], Flynn-Wall-Ozawa [7,8], Kissinger-Akahira-Sunose [9,10] and Kissinger [11] have been used extensively to estimate the kinetic parameters and reaction mechanisms.…”