Abstract:The effects of sample injection time, pH of the buffer solution, micelles concentration and micelles standing time on the peak splitting in MEKC were explored respectively in the research. 4-methyl phenethyl alcohol, 4-methoxy phenethyl alcohol, 4-nitro phenethyl alcohol, benzyl alcohol and phenethyl alcohol were selected as analytes and were separated by CE in a 50 μm i.d. × 60 cm (effective length 45 cm) fused-silica capillary at 20.0 kV. The buffer solution in MEKC consisted of 15.0 mM Na2B4O7, 10.0 mM NaH2… Show more
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