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Cited by 12 publications
(3 citation statements)
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“…2-Bromo-p-xylene (>98.6% pure) was prepared by reacting 0.5 mol of p-xylene with 0.5 mol of Br2 in CC14 (26). It was purified from the reaction mixture by fractional distillation and characterized by gas chromatography (GC) and gas chromatography/mass spectrometry (GC/MS).…”
Section: Methodsmentioning
confidence: 99%
“…We found that compound 6 could be conveniently prepared from 2-bromo-p-xylene. [14] The latter can be either converted to the corresponding Grignard reagent (method A) or lithiated derivative (method B), followed by reaction of the corresponding organometallic intermediate with diethyl chlorophosphate. Compound 6, upon oxidation with KMnO 4 , yields the dipotassium salt of 2-(diethylphosphonyl)terephthalic acid (7).…”
Section: S Branion and V Beninmentioning
confidence: 99%
“…We found that compound 6 could be conveniently prepared from 2-bromo-p-xylene. [14] The latter can be either converted to the corresponding…”
Section: Prepration Of 2-phosphonoterephtahlic Acid (2)mentioning
confidence: 99%