SYNTHESIS OF SOME tert-BUTYLBENZENES RELATED TO SYNTHESIS OF ASYMMETRIC NITRO MUSKS<sup>1</sup>

Burgoyne, E. E.; Klose, T. G.; Watson, D. K.

doi:10.1021/jo01128a008

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S Branion and V Benin1

Prepration Of 2-phosphonoterephtahlic Acid (2)1

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1988

2006

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Cited by 12 publications

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“…2-Bromo-p-xylene (>98.6% pure) was prepared by reacting 0.5 mol of p-xylene with 0.5 mol of Br2 in CC14 (26). It was purified from the reaction mixture by fractional distillation and characterized by gas chromatography (GC) and gas chromatography/mass spectrometry (GC/MS).…”

Section: Methodsmentioning

confidence: 99%

Reactivities of hypochlorous and hypobromous acid, chlorine monoxide, hypobromous acidium ion, chlorine, bromine, and bromine chloride in electrophilic aromatic substitution reactions with p-xylene in water

Voudrias¹,

Reinhard²

1988

Environ. Sci. Technol.

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“…We found that compound 6 could be conveniently prepared from 2-bromo-p-xylene. [14] The latter can be either converted to the corresponding Grignard reagent (method A) or lithiated derivative (method B), followed by reaction of the corresponding organometallic intermediate with diethyl chlorophosphate. Compound 6, upon oxidation with KMnO 4 , yields the dipotassium salt of 2-(diethylphosphonyl)terephthalic acid (7).…”

Section: S Branion and V Beninmentioning

confidence: 99%